Phosphoric acid, diethyl 1-phenyl-2,2-bis(2,4,6-trimethylphenyl)ethenyl ester

Base Information

• Chemical Name: Phosphoric acid, diethyl 1-phenyl-2,2-bis(2,4,6-trimethylphenyl)ethenyl ester
• CAS No.: 184016-72-6
• Molecular Formula: C30H37O4P
• Molecular Weight: 492.595
• Mol file: 184016-72-6.mol

Synonyms:

Chemical Property of Phosphoric acid, diethyl 1-phenyl-2,2-bis(2,4,6-trimethylphenyl)ethenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphoric acid, diethyl 1-phenyl-2,2-bis(2,4,6-trimethylphenyl)ethenyl ester

There total 1 articles about Phosphoric acid, diethyl 1-phenyl-2,2-bis(2,4,6-trimethylphenyl)ethenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

2,2-dimesityl-1-phenylethenol (77787-80-5) + diethyl chlorophosphate (814-49-3) → (2,2-dimesityl-1-phenylethenyl) diethyl phosphate (184016-72-6)

Guidance literature:

2,2-dimesityl-1-phenylethenol; With sodium hydride; In tetrahydrofuran; for 1h;

diethyl chlorophosphate; In tetrahydrofuran; for 19h; Heating;

DOI:10.3891/acta.chem.scand.53-0781

Reference yield: 41.0%

(2,2-dimesityl-1-phenylethenyl) diethyl phosphate (184016-72-6) → 3-mesityl-4,6,7-trimethylbenzofuran

Guidance literature:

With tris(p-nitrophenyl)aminium hexafluoroantimonate; In acetonitrile;

DOI:10.1039/CC9960002349

Reference yield:

(2,2-dimesityl-1-phenylethenyl) diethyl phosphate (184016-72-6) → (2,2-dimesityl-1-phenylethenyl) diethyl phosphate radical cation

Guidance literature:

With O₂⁽¹⁺⁾*AsF₆^(1-)=(O₂)AsF₆; In Chlorodifluoromethane; at -100 ℃;

DOI:10.1039/CC9960002349

upstream raw materials:

2,2-dimesityl-1-phenylethenol

diethyl chlorophosphate