1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose

Base Information

• Chemical Name: 1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose
• CAS No.: 97614-41-0
• Molecular Formula: C27H21 F3 O10 S
• Molecular Weight: 594.519
• Hs Code.: 29400090
• Mol file: 97614-41-0.mol

Synonyms:a-D-Ribofuranose,1,3,5-tribenzoate 2-(trifluoromethanesulfonate) (9CI);

Chemical Property of 1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose

Chemical Property:

• Vapor Pressure: 1.42E-16mmHg at 25°C
• Refractive Index: 1.594
• Boiling Point: 646°Cat760mmHg
• Flash Point: 344.5°C
• PSA: 139.88000
• Density: 1.5g/cm³
• LogP: 4.96650

Purity/Quality:

99%, ^*data from raw suppliers

1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose is a furanose used in the production of positron-?emission tomography (PET) probes.

Technology Process of 1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose

There total 1 articles about 1,3,5-Tri-O-benzoyl-2-O-(trifluoromethanesulfonyl)-a-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

trifluoromethylsulfonic anhydride (358-23-6) + 1,3,5-tri-O-benzoyl-α-D-ribofuranoside (22224-41-5) → 2-O-<(trifluoromethyl)sulfonyl>-1,3,5-tri-O-benzoyl-α-D-ribofuranose (97614-41-0)

Guidance literature:

In pyridine; dichloromethane; at -10 ℃;

DOI:10.1016/S0040-4020(98)00460-8

Reference yield: 96.0%

2-O-<(trifluoromethyl)sulfonyl>-1,3,5-tri-O-benzoyl-α-D-ribofuranose (97614-41-0) → C26H21BrO7

Guidance literature:

With lithium bromide; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/op800182x

Reference yield: 92.3%

cesium acetate (3396-11-0) + 2-O-<(trifluoromethyl)sulfonyl>-1,3,5-tri-O-benzoyl-α-D-ribofuranose (97614-41-0) → 2-O-Acetyl-1,3,5-tri-O-benzoyl-α-D-arabinofuranose

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 3h;

DOI:10.1021/acs.orglett.6b02675

upstream raw materials:

trifluoromethylsulfonic anhydride

1,3,5-tri-O-benzoyl-α-D-ribofuranoside

Downstream raw materials:

1,3,5-tri-O-benzoyl-2-deoxy-2-fluoro-α-D-arabinofuranose

(2R,3S,4R,5R)-5-((benzoyloxy)methyl)-3-[¹⁸F]fluoro-tetrahydrofuran-2,4-diyl dibenzoate

1-bromo-2-deoxy-2-[18F]fluoro-3,5-di-O-benzoyl-α-D-arabinofuranose

((2R,3R,4S)-3-(benzoyloxy)-5-bromo-4-fluorotetrahydrofuran-2-yl)methyl benzoate

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