Benzoic acid, 2-heptyl-4-[[2-hydroxy-4-methoxy-6-(2-oxononyl)benzoyl]oxy]-6-methoxy- , phenylmethyl ester

Base Information

Chemical Name:Benzoic acid, 2-heptyl-4-[[2-hydroxy-4-methoxy-6-(2-oxononyl)benzoyl]oxy]-6-methoxy- , phenylmethyl ester
CAS No.:184375-13-1
Molecular Formula:C39H50O8
Molecular Weight:646.821
Hs Code.:
Mol file:184375-13-1.mol

Synonyms:

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Chemical Property of Benzoic acid, 2-heptyl-4-[[2-hydroxy-4-methoxy-6-(2-oxononyl)benzoyl]oxy]-6-methoxy- , phenylmethyl ester

Chemical Property:

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Technology Process of Benzoic acid, 2-heptyl-4-[[2-hydroxy-4-methoxy-6-(2-oxononyl)benzoyl]oxy]-6-methoxy- , phenylmethyl ester

There total 10 articles about Benzoic acid, 2-heptyl-4-[[2-hydroxy-4-methoxy-6-(2-oxononyl)benzoyl]oxy]-6-methoxy- , phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 184375-08-4
benzyl superconfluentate ethylene ketal

: 184375-13-1
benzyl superconfluentate

Guidance literature:: With hydrogenchloride; In methanol; for 2h; Ambient temperature;
DOI:10.1071/ch9960917

Reference yield:

: 13195-66-9
ethyl 3-oxodecanoate

: 184375-13-1
benzyl superconfluentate

Guidance literature:: Multi-step reaction with 10 steps

1: 82 percent / p-toluenesulfonic acid / toluene / 5 h / Heating

2: 90 percent / LiAlH₄ / diethyl ether / 4 h / Heating

3: 81 percent / pyridinium dichromate / CH₂Cl₂ / 22 h / Heating

4: 48 percent / toluene / 21 h / 50 °C

5: 1.) sodium, ethanol / 1.) r.t., 30 min, 2.) ethanol, reflux, 24 h

7: 97 percent / diethyl ether / 16 h / Ambient temperature

8: 86 percent / sodium hydroxide / H₂O; dimethylsulfoxide / 17 h / 93 °C

9: 59 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature

10: 86 percent / 5M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; dipyridinium dichromate; ethanol; sodium; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1071/ch9960917

Reference yield:

: 161838-89-7
2-(2-hydroxyethyl)-2-heptyl-1,3-dioxolane

: 184375-13-1
benzyl superconfluentate

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / pyridinium dichromate / CH₂Cl₂ / 22 h / Heating

2: 48 percent / toluene / 21 h / 50 °C

3: 1.) sodium, ethanol / 1.) r.t., 30 min, 2.) ethanol, reflux, 24 h

5: 97 percent / diethyl ether / 16 h / Ambient temperature

6: 86 percent / sodium hydroxide / H₂O; dimethylsulfoxide / 17 h / 93 °C

7: 59 percent / N,N-dicyclohexylcarbodiimide / toluene / Ambient temperature

8: 86 percent / 5M HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; dipyridinium dichromate; ethanol; sodium; dicyclohexyl-carbodiimide; In methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1071/ch9960917