Acridine, 9,10-dihydro-10-propyl-

Base Information

• Chemical Name: Acridine, 9,10-dihydro-10-propyl-
• CAS No.: 18448-45-8
• Molecular Formula: C16H17N
• Mol file: 18448-45-8.mol

Synonyms:

Chemical Property of Acridine, 9,10-dihydro-10-propyl-

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acridine, 9,10-dihydro-10-propyl-

There total 3 articles about Acridine, 9,10-dihydro-10-propyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

N(-n-propyl)acridine-9-one (60536-17-6) → N-Propyl-acridan (18448-45-8)

Guidance literature:

With sodium; In pentan-1-ol; Heating;

DOI:10.1021/je00055a038

Reference yield: 54.0%

acridine (92-81-9) + propyl bromide (106-94-5) → N-Propyl-acridan (18448-45-8)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c2cc30684k

Reference yield:

10H-acridin-9-one (578-95-0,790240-54-9) → N-Propyl-acridan (18448-45-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 50percent aq. NaOH / triethylbenzylammonium chloride / butan-2-one / 2 h / Heating

2: 74 percent / Na / pentan-1-ol / Heating

With sodium hydroxide; sodium; N-benzyl-N,N,N-triethylammonium chloride; In pentan-1-ol; butanone;

DOI:10.1021/je00055a038

upstream raw materials:

N(-n-propyl)acridine-9-one

10H-acridin-9-one

acridine

propyl bromide