Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester

Base Information

Chemical Name:Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester
CAS No.:184592-21-0
Molecular Formula:C59H49NO10
Molecular Weight:932.039
Hs Code.:
Mol file:184592-21-0.mol

Benzoic acid,
3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon
yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester

Synonyms:

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Chemical Property of Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester

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Technology Process of Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester

There total 3 articles about Benzoic acid, 3,5-bis(phenylmethoxy)-4-[2-(phenylmethoxy)-6-[(phenylmethoxy)carbon yl]benzoyl]-, 2-[[4-(phenylmethoxy)benzoyl]amino]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 167832-93-1
3-Benzyloxy-2-(2,6-bis-benzyloxy-4-chlorocarbonyl-benzoyl)-benzoic acid benzyl ester

: 122053-75-2
4-benzyloxy-N-(2-hydroxy-ethyl)-benzamide

: 184592-21-0
benzyl 2-[(4-{[2-({[4-(benzyloxy)phenyl]carbonyl}amino)ethoxy]carbonyl}-2,6-bis(benzyloxy)phenyl)carbonyl]-3-(benzyloxy)benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jm960581w

Reference yield:

: 1486-50-6
4-(benzyloxy)benzoic acid chloride

: 184592-21-0
benzyl 2-[(4-{[2-({[4-(benzyloxy)phenyl]carbonyl}amino)ethoxy]carbonyl}-2,6-bis(benzyloxy)phenyl)carbonyl]-3-(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / KOH / tetrahydrofuran / 4 h / Ambient temperature

2: 86 percent / Et₃N, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

With dmap; potassium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm960581w

Reference yield:

: 158585-06-9
4-(6-Benzyloxy-2-(benzyloxycarbonyl)benzoyl)-3,5-dibenzyloxybenzoic Acid

: 184592-21-0
benzyl 2-[(4-{[2-({[4-(benzyloxy)phenyl]carbonyl}amino)ethoxy]carbonyl}-2,6-bis(benzyloxy)phenyl)carbonyl]-3-(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 2 h / Ambient temperature

2: 86 percent / Et₃N, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

With dmap; oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm960581w