Silane, [3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]- 3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl-

Base Information

Chemical Name:Silane, [3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]- 3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl-
CAS No.:184969-90-2
Molecular Formula:C28H34Cl2F6O2S2Si
Molecular Weight:679.691
Hs Code.:

Silane,
[3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]-
3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl-

Synonyms:

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Chemical Property of Silane, [3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]- 3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl-

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Technology Process of Silane, [3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]- 3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl-

There total 4 articles about Silane, [3-[2-[[[3,5-bis(trifluoromethyl)phenyl]methoxy]methyl]-1,3-dithiolan-2-yl]- 3-(3,4-dichlorophenyl)propoxy](1,1-dimethylethyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 32247-96-4
3,5-bis(trifluoromethyl)benzyl bromide

: 184969-89-9
{2-[3-(tert-butyl-dimethyl-silanyloxy)-1-(3,4-dichloro-phenyl)-propyl]-[1,3]dithiolan-2-yl}-methanol

: 184969-90-2
[3-[2-(3,5-bis-trifluoromethyl-benzyloxymethyl)-[1,3]dithiolan-2-yl]-3-(3,4-dichloro-phenyl)-propoxy]-tert-butyl-dimethyl-silane

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at 0 - 23 ℃;
DOI:10.1016/S0960-894X(00)00464-9

Reference yield:

: 82475-75-0
methyl 3-(3,4-dichlorophenyl)-2-propenoate

: 184969-90-2
[3-[2-(3,5-bis-trifluoromethyl-benzyloxymethyl)-[1,3]dithiolan-2-yl]-3-(3,4-dichloro-phenyl)-propoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / LiN(TMS)2 / tetrahydrofuran / -78 °C

2: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 23 °C

3: 96 percent / Et₃N; DMAP / tetrahydrofuran / 0 - 23 °C

4: 88 percent / KN(TMS)2 / tetrahydrofuran / 0 - 23 °C

With dmap; lithium aluminium tetrahydride; potassium hexamethylsilazane; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; 1: Addition / 2: Reduction / 3: silylation / 4: Alkylation;
DOI:10.1016/S0960-894X(00)00464-9

Reference yield:

: 184969-87-7
3-(3,4-dichloro-phenyl)-3-(2-hydroxymethyl-[1,3]dithiolan-2-yl)-propan-1-ol

: 184969-90-2
[3-[2-(3,5-bis-trifluoromethyl-benzyloxymethyl)-[1,3]dithiolan-2-yl]-3-(3,4-dichloro-phenyl)-propoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N; DMAP / tetrahydrofuran / 0 - 23 °C

2: 88 percent / KN(TMS)2 / tetrahydrofuran / 0 - 23 °C

With dmap; potassium hexamethylsilazane; triethylamine; In tetrahydrofuran; 1: silylation / 2: Alkylation;
DOI:10.1016/S0960-894X(00)00464-9