2,5-Diiodo-4-methylimidazole

Base Information

• Chemical Name: 2,5-Diiodo-4-methylimidazole
• CAS No.: 149510-85-0
• Molecular Formula: C₄H₄I₂N₂
• Molecular Weight: 333.898
• Hs Code.: 2933290090
• Mol file: 149510-85-0.mol

Synonyms:1H-Imidazole,2,4-diiodo-5-methyl- (9CI); 2,4-Diiodo-5-methylimidazole; NSC 280627

Chemical Property of 2,5-Diiodo-4-methylimidazole

Chemical Property:

• Appearance/Colour: crystal
• Vapor Pressure: 3.4E-06mmHg at 25°C
• Boiling Point: 387 °C at 760 mmHg
• Flash Point: 187.8 °C
• PSA: 28.68000
• Density: 2.75 g/cm³
• LogP: 1.92730
• Storage Temp.: Sealed in dry,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

2,5-Diiodo-4-methyl-1H-imidazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-Diiodo-4-methylimidazole

There total 3 articles about 2,5-Diiodo-4-methylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

→ 2,5-diiodo-4-methyl-1H-imidazole (149510-85-0)

Guidance literature:

With N-iodo-succinimide; In acetonitrile; at 80 ℃; for 16h;

Reference yield:

4-methyl-1H-imidazole (822-36-6) → 2,5-diiodo-4-methyl-1H-imidazole (149510-85-0)

Guidance literature:

With iodine; periodic acid; In ethanol; at 60 ℃; Inert atmosphere;

DOI:10.1002/ejoc.202100632

Reference yield:

4-methyl-1H-imidazole (822-36-6) → 2,4-diiodo-5-methyl-1(3)H-imidazole (149510-85-0)

Guidance literature:

With iodine; sodium carbonate;

upstream raw materials:

4-methyl-1H-imidazole

Downstream raw materials:

5-iodo-4-methyl-1H-imidazole

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