1,1'-Binorbornane

Base Information

• Chemical Name: 1,1'-Binorbornane
• CAS No.: 18313-42-3
• Molecular Formula: C14H22
• Molecular Weight: 190.329
• NSC Number: 102307
• DSSTox Substance ID: DTXSID801308926
• Nikkaji Number: J1.926.645A
• Mol file: 18313-42-3.mol

Synonyms:1,1'-Binorbornane;1,1'-Bibicyclo[2.2.1]heptane;18313-42-3;NSC102307;1,1'-Bis(bicyclo[2.2.1]heptane);DTXSID801308926;NSC-102307

Chemical Property of 1,1'-Binorbornane

Chemical Property:

• Boiling Point: 253.6°Cat760mmHg
• Flash Point: 93.1°C
• Density: 1.096g/cm³
• XLogP3: 5.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 190.172150702
• Heavy Atom Count: 14
• Complexity: 221

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2(CCC1C2)C34CCC(C3)CC4

Technology Process of 1,1'-Binorbornane

There total 10 articles about 1,1'-Binorbornane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,4-diiodobicyclo<2.2.1>heptane (40950-21-8) + mercury → norbornene (279-23-2) + 1,1'-binorbornane (18313-42-3) + bis(1-norbornyl)mercury (67773-54-0)

Guidance literature:

With tetramethylammonium perchlorate; In N,N-dimethyl-formamide; Electrolysis; at 25°C, at mercury cathode, at -1.6 V;

DOI:10.1021/ja00532a024

Reference yield: 60.0%

1,4-dibromobicyclo<2.2.1>heptane (40950-22-9) + mercury → norbornene (279-23-2) + 1,1'-binorbornane (18313-42-3) + bis(1-norbornyl)mercury (67773-54-0)

Guidance literature:

With tetra-n-butylammonium perchlorate; In N,N-dimethyl-formamide; Electrolysis; at -34°C, at mercury cathode, at -2.1 V;

DOI:10.1021/ja00532a024

Reference yield: 60.0%

1,4-diiodobicyclo<2.2.1>heptane (40950-21-8) + mercury → tributyl-amine (102-82-9) + norbornene (279-23-2) + 1,1'-binorbornane (18313-42-3) + bis(1-norbornyl)mercury (67773-54-0)

Guidance literature:

With tetra-n-butylammonium perchlorate; In N,N-dimethyl-formamide; Electrolysis; at 25°C, at mercury cathode, at -1.9 V;

DOI:10.1021/ja00532a024

upstream raw materials:

trans-2,3-diazabicyclo<2.2.1>hept-2-ene

1,4-dibromobicyclo<2.2.1>heptane

1,4-diiodobicyclo<2.2.1>heptane

cis-2,3-diazabicyclo<2.2.1>hept-2-ene

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