5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)-

Base Information

Chemical Name:5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)-
CAS No.:185434-98-4
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:
Mol file:185434-98-4.mol

Synonyms:

Suppliers and Price of 5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)-

There total 7 articles about 5-Decenoic acid, 8-benzoyl-9-oxo-, ethyl ester, (5Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64084-55-5
1-bromo-6-<(tetrahydro-2H-pyran-2-yl)oxy>-4-hexyne

: 185434-98-4
(Z)-8-Benzoyl-9-oxo-dec-5-enoic acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / dimethylsulfoxide / 20 h / 45 °C

2: 78 percent / Dowex 50W-X₈ / methanol / 11 h / Ambient temperature

3: 87 percent / H₂, NaBH₄, Ni(OAc)2*4H₂O, ethylenediamine / methanol / 24 h / Ambient temperature

4: NaOH / methanol; H₂O / 24 h / Heating

5: BF₃*OEt₂ / 3 h / 60 °C

6: 76 percent / CBr₄, Ph₃P / CH₂Cl₂ / 1 h / Ambient temperature

7: 1.) K₂CO₃, Bu₄NBr / 1.) toluene, 100 deg C, 3 h, 2.) toluene, 40 deg C, 14 h

With sodium hydroxide; sodium tetrahydroborate; carbon tetrabromide; Dowex 50W-X₈; boron trifluoride diethyl etherate; tetrabutylammomium bromide; hydrogen; nickel diacetate; potassium carbonate; ethylenediamine; triphenylphosphine; In methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/jo9616365

Reference yield:

: 34506-48-4
6-<(tetrahydropyranyl)oxy>-4-hexynenitrile

: 185434-98-4
(Z)-8-Benzoyl-9-oxo-dec-5-enoic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / Dowex 50W-X₈ / methanol / 11 h / Ambient temperature

2: 87 percent / H₂, NaBH₄, Ni(OAc)2*4H₂O, ethylenediamine / methanol / 24 h / Ambient temperature

3: NaOH / methanol; H₂O / 24 h / Heating

4: BF₃*OEt₂ / 3 h / 60 °C

5: 76 percent / CBr₄, Ph₃P / CH₂Cl₂ / 1 h / Ambient temperature

6: 1.) K₂CO₃, Bu₄NBr / 1.) toluene, 100 deg C, 3 h, 2.) toluene, 40 deg C, 14 h

With sodium hydroxide; sodium tetrahydroborate; carbon tetrabromide; Dowex 50W-X₈; boron trifluoride diethyl etherate; tetrabutylammomium bromide; hydrogen; nickel diacetate; potassium carbonate; ethylenediamine; triphenylphosphine; In methanol; dichloromethane; water;
DOI:10.1021/jo9616365

Reference yield:

: 69160-15-2
(Z)-ethyl 7-hydroxyhept-5-enoate

: 185434-98-4
(Z)-8-Benzoyl-9-oxo-dec-5-enoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / CBr₄, Ph₃P / CH₂Cl₂ / 1 h / Ambient temperature

2: 1.) K₂CO₃, Bu₄NBr / 1.) toluene, 100 deg C, 3 h, 2.) toluene, 40 deg C, 14 h

With carbon tetrabromide; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; In dichloromethane;
DOI:10.1021/jo9616365