Germane, triphenyl-2-propenyl-

Base Information

Chemical Name:Germane, triphenyl-2-propenyl-
CAS No.:18689-08-2
Molecular Formula:C21H20Ge
Molecular Weight:344.98
Hs Code.:
DSSTox Substance ID:DTXSID70400674
Nikkaji Number:J496.484E
Wikidata:Q82203685

Synonyms:Allyltriphenylgermane;Germane, triphenyl-2-propenyl-;18689-08-2;Triphenyl(2-propenyl)germane;DTXSID70400674;OCYWVANHJJNAKH-UHFFFAOYSA-N;AKOS024338777

Suppliers and Price of Germane, triphenyl-2-propenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Germane, triphenyl-2-propenyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:346.0776784
Heavy Atom Count:22
Complexity:284

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC[Ge](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Germane, triphenyl-2-propenyl-

There total 5 articles about Germane, triphenyl-2-propenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1626-24-0
chlorotriphenylgermane

: 1730-25-2
allylmagnesium bromide

: 18689-08-2
monoallyl(triphenyl)germane

Guidance literature:: In diethyl ether; 0°C or room temp.;
DOI:10.1246/cl.2011.967

Reference yield: 88.0%

: 463-49-0
1,2-propanediene

: 2816-43-5
triphenylgermane

: 18689-08-2
monoallyl(triphenyl)germane

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Ar atmosphere, stirring (25°C, 5 h); pouring of reaction mixt. into water, extraction (ethyl acetate), drying of combined extracts (Na2SO4), concn. (vacuum), chromy. (TLC, silica gel);
DOI:10.1246/bcsj.61.2693