2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine

Base Information

Chemical Name:2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine
CAS No.:18725-60-5
Molecular Formula:C10Cl8N2
Molecular Weight:431.747
Hs Code.:
DSSTox Substance ID:DTXSID80500715
Wikidata:Q82352569

Synonyms:18725-60-5;octachloro-4,4'-bipyridyl;2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine;DTXSID80500715

Suppliers and Price of 2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine

Chemical Property:

XLogP3:7.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:431.751069
Heavy Atom Count:20
Complexity:287

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1(=C(C(=NC(=C1Cl)Cl)Cl)Cl)C2=C(C(=NC(=C2Cl)Cl)Cl)Cl

Technology Process of 2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine

There total 8 articles about 2,2',3,3',5,5',6,6'-Octachloro-4,4'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 23995-94-0
4-Bromo-2,3,5,6-tetrachloropyridine

: 2402-79-1
2,3,5,6-tetrachloropyridine

: 14121-36-9
2,3,4,6-Tetrachloropyridine

: octachloro-3,4'-bipyridyl

: 18725-60-5
octachloro-4,4'-bipyridyl

Guidance literature:: With copper; benzoyl chloride; In N,N-dimethyl-formamide; at 150 ℃; for 0.5h;
DOI:10.1039/P19800001682

Reference yield: 18.0%

: 23995-94-0
4-Bromo-2,3,5,6-tetrachloropyridine

: 2402-79-1
2,3,5,6-tetrachloropyridine

: 14121-36-9
2,3,4,6-Tetrachloropyridine

: 2176-62-7
2,3,4,5,6-pentachloropyridine

: octachloro-3,4'-bipyridyl

: 18725-60-5
octachloro-4,4'-bipyridyl

Guidance literature:: With para-xylene; copper; In N,N-dimethyl-formamide; at 150 ℃; for 1h; Product distribution; Mechanism; the similar reaction without p-xylene; in presence cumene, benzoyl chloride instead p-xylene; other reagent (CuCl); other polychloroiodoarenes; tetrahalohenopyridylcopper intermediate; evidence against free radical or pyridyne intermediates;
DOI:10.1039/P19800001682

Reference yield: 16.0%

: 23995-94-0
4-Bromo-2,3,5,6-tetrachloropyridine

: 2402-79-1
2,3,5,6-tetrachloropyridine

: 14121-36-9
2,3,4,6-Tetrachloropyridine

: 2176-62-7
2,3,4,5,6-pentachloropyridine

: 18725-60-5
octachloro-4,4'-bipyridyl

Guidance literature:: With Isopropylbenzene; copper; In N,N-dimethyl-formamide; at 150 ℃; for 1h; Further byproducts given;
DOI:10.1039/P19800001682