Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-

Base Information

Chemical Name:Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-
CAS No.:106710-59-2
Molecular Formula:C₁₁H₁₀O
Molecular Weight:158.2
Hs Code.:
DSSTox Substance ID:DTXSID50910100
Wikidata:Q82879852
Mol file:106710-59-2.mol

Synonyms:106710-59-2;Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-;Bicyclo[2.2.1]heptan-7-one, 2,3,5,6-tetramethylene-;2,3,5,6-tetramethylidenebicyclo[2.2.1]heptan-7-one;DTXSID50910100

Suppliers and Price of Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-

Chemical Property:

Vapor Pressure:0.0156mmHg at 25°C
Melting Point:56-57 °C(Solv: pentane (109-66-0))
Boiling Point:256.2°Cat760mmHg
Flash Point:103.9°C
PSA：17.07000
Density:1.04g/cm³
LogP:2.03990
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:158.073164938
Heavy Atom Count:12
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C1C2C(=C)C(=C)C(C1=C)C2=O

Technology Process of Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene-

There total 19 articles about Bicyclo(2.2.1)heptan-7-one, 2,3,5,6-tetramethylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 136846-80-5
2,3,5,6-Tetramethylene-bicyclo[2.2.1]heptan-7-ol

: 106710-59-2
2,3,5,6-tetramethylidene-2-bicyclo<2.2.1>heptanone

Guidance literature:: With oxallyl chloride; triethylamine; In dichloromethane; dimethyl sulfoxide; at -78 ℃;

Reference yield: 48.0%

: 120567-60-4
7-(2'-hydroxypropan-2'-yl)-2,3,5,6-tetramethylidenebicyclo<2.2.1>heptan-2-ol

: 106710-59-2
2,3,5,6-Tetramethylen-7-norbornanon

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/hlca.19880710538

Reference yield:

: 2175-91-9
6,6'-dimethyl fulvene

: 106710-59-2
2,3,5,6-tetramethylidene-2-bicyclo<2.2.1>heptanone

Guidance literature:: Multi-step reaction with 6 steps

2: 70 percent / 1) CuCl / 10percent Pd/C / 3 h / 60 °C / 3800 Torr

3: 70 percent / K₂CO₃ / methanol / 20 °C

6: 90 percent / oxallyl chloride, NEt₃ / CH₂Cl₂; dimethylsulfoxide / -78 °C

With oxallyl chloride; potassium carbonate; triethylamine; copper(l) chloride; palladium on activated charcoal; In methanol; dichloromethane; dimethyl sulfoxide;