8,9-Dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

Base Information

Chemical Name:8,9-Dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride
CAS No.:69739-51-1
Molecular Formula:
Molecular Weight:0
Hs Code.:

Synonyms:

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Chemical Property of 8,9-Dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

Chemical Property:

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Safty Information:

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Technology Process of 8,9-Dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

There total 7 articles about 8,9-Dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57987-75-4
N-<(2,3-dichlorophenyl)methylene>-2,2-dimethoxyethanamine

: 69739-51-1
8,9-dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 59 percent / H₂ / PtO₂ / ethyl acetate / 1 h / 1034.3 Torr

2: 79 percent / AlCl₃ / CH₂Cl₂ / 0.17 h / Ambient temperature

3: 85 percent / NaOH, benzyltriethylammonium chloride / 6 h / Ambient temperature

4: 30 percent / 6 h / Heating

5: H₂ / PtO₂ / methanol / 760 Torr / Ambient temperature

6: aq. HCl / Heating

With hydrogenchloride; sodium hydroxide; aluminium trichloride; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; platinum(IV) oxide; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo01298a038

Reference yield:

: 73261-85-5
2-acetyl-7,8-dichloro-1,2-dihydroisoquinoline

: 69739-51-1
8,9-dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / NaOH, benzyltriethylammonium chloride / 6 h / Ambient temperature

2: 30 percent / 6 h / Heating

3: H₂ / PtO₂ / methanol / 760 Torr / Ambient temperature

4: aq. HCl / Heating

With hydrogenchloride; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; platinum(IV) oxide; In methanol;
DOI:10.1021/jo01298a038

Reference yield:

: 73261-79-7
N-(2,3-dichlorobenzyl)-N-(2,2-dimethoxyethyl)acetamide

: 69739-51-1
8,9-dichloro-2,3,4,5-tetrahydro-1H-2-benzazepine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / AlCl₃ / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 85 percent / NaOH, benzyltriethylammonium chloride / 6 h / Ambient temperature

3: 30 percent / 6 h / Heating

4: H₂ / PtO₂ / methanol / 760 Torr / Ambient temperature

5: aq. HCl / Heating

With hydrogenchloride; sodium hydroxide; aluminium trichloride; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; platinum(IV) oxide; In methanol; dichloromethane;
DOI:10.1021/jo01298a038