2-butyl-3-(dimethylamino)-2-ethyl-4,4-dimethylcyclobutanol

Base Information

• Chemical Name: 2-butyl-3-(dimethylamino)-2-ethyl-4,4-dimethylcyclobutanol
• CAS No.: 14241-13-5
• Molecular Formula: C₁₄H₂₉NO
• Molecular Weight: 227.39
• Mol file: 14241-13-5.mol

Synonyms:RP 1918

Chemical Property of 2-butyl-3-(dimethylamino)-2-ethyl-4,4-dimethylcyclobutanol

Chemical Property:

• Vapor Pressure: 0.00025mmHg at 25°C
• Boiling Point: 289°Cat760mmHg
• Flash Point: 95°C
• Density: 0.92g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-butyl-3-(dimethylamino)-2-ethyl-4,4-dimethylcyclobutanol

There total 2 articles about 2-butyl-3-(dimethylamino)-2-ethyl-4,4-dimethylcyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Dimethylamino-2,2-dimethyl-4-aethyl-4-butyl-cyclobutanon (1139-20-4) → 3-Dimethylamino-4,4-dimethyl-2-aethyl-2-butyl-cyclobutanol (14241-13-5)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jo01041a007

Reference yield:

C10H21N → 3-Dimethylamino-4,4-dimethyl-2-aethyl-2-butyl-cyclobutanol (14241-13-5)

Guidance literature:

Multi-step reaction with 2 steps

1: AcOiPr

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; Isopropyl acetate; In diethyl ether;

DOI:10.1021/jo01041a007

upstream raw materials:

3-Dimethylamino-2,2-dimethyl-4-aethyl-4-butyl-cyclobutanon