Technology Process of 6-Phenylhex-1-ene-3,4-diol
There total 5 articles about 6-Phenylhex-1-ene-3,4-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
acetic acid 3-bromo-1-propenyl ester;
With
indium;
In
tetrahydrofuran;
at 0 - 25 ℃;
for 4h;
3-phenyl-propionaldehyde;
In
tetrahydrofuran;
at 0 ℃;
for 4h;
With
potassium carbonate;
In
methanol; water;
at 25 ℃;
Further stages.;
DOI:10.1021/jo0262457
- Guidance literature:
-
With
ammonia; toluene-4-sulfonic acid;
In
neat (no solvent);
at 80 ℃;
for 72h;
Product distribution;
in sealed tube; aminolysis also with amines; various vinylepoxides, substituent effect; stereo- and regioselectivity studied;
DOI:10.1016/S0040-4039(97)00224-4
- Guidance literature:
-
(E)-1-phenylhex-4-en-3-ol;
With
oxygen; 5,15,10,20-tetraphenylporphyrin;
In
tetrachloromethane;
at 0 ℃;
Irradiation;
With
triphenylphosphine;
In
tetrachloromethane;
at 0 ℃;
Further stages.;
DOI:10.1016/j.tetlet.2004.03.157