1-[(methylsulfonyl)methyl]-4-nitrobenzene

Base Information

Chemical Name:1-[(methylsulfonyl)methyl]-4-nitrobenzene
CAS No.:61081-34-3
Molecular Formula:C8H9NO4S
Molecular Weight:215.23
Hs Code.:2904909090
Mol file:61081-34-3.mol

Synonyms:1-[(methylsulphonyl)methyl]-4-nitrobenzene;2-bromo-4-nitro-benzoic acid;<<(4-nitrophenyl)methyl>sulphonyl>methane;Methyl-(4-nitro-benzyl)-sulfon;methyl 4-nitro-2-bromobenzoic acid;o-bromo-p-nitrobenzoic acid;methyl-(4-nitro-benzyl)-sulfone;2-Brom-4-nitro-benzoesaeure;

Suppliers and Price of 1-[(methylsulfonyl)methyl]-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(Methanesulfonylmethyl)-4-nitrobenzene 95+%
25g
$ 452.00

Total 7 raw suppliers

Chemical Property of 1-[(methylsulfonyl)methyl]-4-nitrobenzene

Chemical Property:

Vapor Pressure:3.37E-08mmHg at 25°C
Boiling Point:459.8°Cat760mmHg
Flash Point:231.9°C
PSA：88.34000
Density:1.387g/cm³
LogP:2.74340

Purity/Quality:

99% ^*data from raw suppliers

1-(Methanesulfonylmethyl)-4-nitrobenzene 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-[(methylsulfonyl)methyl]-4-nitrobenzene

There total 15 articles about 1-[(methylsulfonyl)methyl]-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 619-73-8
4-nitrobenzyl chloride

: 20277-69-4
sodium methansulfinate

: 61081-34-3
methyl 4-nitrobenzylsulfone

Guidance literature:: With boron trifluoride diethyl etherate; acetic acid; at 20 ℃;
DOI:10.3906/KIM-2003-10

Reference yield: 93.0%

: 20277-69-4
sodium methansulfinate

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 61081-34-3
methyl 4-nitrobenzylsulfone

Guidance literature:: In N,N-dimethyl-formamide; at 65 ℃; for 1h;

Reference yield: 78.0%

: 104-03-0
4-nitrobenzeneacetic acid

: 20277-69-4
sodium methansulfinate

: 61081-34-3
methyl 4-nitrobenzylsulfone

Guidance literature:: With copper(II) acetate monohydrate; In N,N-dimethyl-formamide; at 115 ℃; for 6h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02516