trans-2,2-DiMethyl-6-hydroxy-5-aMino-1,3-dioxepane

Base Information

• Chemical Name: trans-2,2-DiMethyl-6-hydroxy-5-aMino-1,3-dioxepane
• CAS No.: 188923-20-8
• Molecular Formula: C7H15NO3
• Molecular Weight: 161.201
• Mol file: 188923-20-8.mol

Synonyms:trans-5-amino-2,2-dimethyl-6-hydroxy-1,3-dioxepane;trans-6-amino-2,2-dimethyl-1,3-dioxepan-5-ol;trans-5-amino-2,2-dimethyl-6-hydroxy-1,3-dioxepan;

Chemical Property of trans-2,2-DiMethyl-6-hydroxy-5-aMino-1,3-dioxepane

Chemical Property:

• PSA: 64.71000
• LogP: 0.15780

Purity/Quality:

95% Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-2,2-DiMethyl-6-hydroxy-5-aMino-1,3-dioxepane

There total 1 articles about trans-2,2-DiMethyl-6-hydroxy-5-aMino-1,3-dioxepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane (57280-22-5) → trans-2,2-Dimethyl-6-hydroxy-5-amino-1,3-dioxepane (188923-20-8,79944-37-9)

Guidance literature:

With ammonia; In water;

Reference yield: 99.0%

3-(N-2,3-Diacetoxypropylacetamido)-5-(N-methyl-acetamido)-2,4,6-triiodobenzoyl chloride (31122-80-2) + trans-2,2-Dimethyl-6-hydroxy-5-amino-1,3-dioxepane (188923-20-8,79944-37-9) → 3-N-2,3-Diacetoxypropylacetamido)-5-(N-methyl-acetamido)-2,4,6-triiodobenzoyl chloride + 3-(N-2,3-Diacetoxypropylacetamido)-5-(N-methyl-acetamido)-2,4,6-triiodo-N-(trans-2,2-dimethyl-6-hydroxy-1,3-dioxepan-5-yl)-benzamide

Guidance literature:

With triethylamine; In dichloromethane; ISOPROPYLAMIDE;

Reference yield:

5-(N-2,3-Diacetoxypropylacetamido)-2,4,6-triiodo-N-methylisophthalamic acid chloride (111453-27-1) + trans-2,2-Dimethyl-6-hydroxy-5-amino-1,3-dioxepane (188923-20-8,79944-37-9) → 5-(N-2,3-Diacetoxypropylacetamido)-2,4,6-triiodo-N-(trans-2,2-dimethyl-6-hydroxy-1,3-dioxepan-5-yl)-N'-methylisophthalamide

Guidance literature:

With trimethylamine; In ISOPROPYLAMIDE; ethyl acetate;

upstream raw materials:

4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

Downstream raw materials:

Methanesulfonic acid (5R,6S)-6-benzoylamino-2,2-dimethyl-[1,3]dioxepan-5-yl ester

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