(4-Chlorophenyl)phosphonothioic dichloride

Base Information

• Chemical Name: (4-Chlorophenyl)phosphonothioic dichloride
• CAS No.: 3064-55-9
• Molecular Formula: C6H4 Cl3 P S
• Molecular Weight: 245.497
• NSC Number: 176340
• DSSTox Substance ID: DTXSID20306430
• Wikidata: Q82053531
• Mol file: 3064-55-9.mol

Synonyms:3064-55-9;NSC176340;(4-chlorophenyl)phosphonothioic dichloride;DTXSID20306430;NSC-176340;Phosphonothioic dichloride, (4-chlorophenyl)-

Chemical Property of (4-Chlorophenyl)phosphonothioic dichloride

Chemical Property:

• Vapor Pressure: 0.00207mmHg at 25°C
• Boiling Point: 299.9°Cat760mmHg
• Flash Point: 135.2°C
• Density: 1.54g/cm³
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 243.883691
• Heavy Atom Count: 11
• Complexity: 171

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1P(=S)(Cl)Cl)Cl

Technology Process of (4-Chlorophenyl)phosphonothioic dichloride

There total 1 articles about (4-Chlorophenyl)phosphonothioic dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-chlorophenylphosphorothioic dichloride (3064-55-9)

Guidance literature:

4-Chlor-phenyl-dichlor-phosphin, S, AlCl3;

Reference yield: 57.0%

2,2'-dihydroxybiphenyl (1806-29-7) + 4-chlorophenylphosphorothioic dichloride (3064-55-9) → 6-(4-chlorophenoxy)dibenzo<1,3,2>dioxaphosphepin 6-sulphide

Guidance literature:

With Et N; In benzene; for 6h; Heating;

DOI:10.1002/mrc.1260260518