Technology Process of 2-Propanol, 1-amino-3-(3-methylphenoxy)-, (2S)-
There total 8 articles about 2-Propanol, 1-amino-3-(3-methylphenoxy)-, (2S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
under 760.051 Torr;
DOI:10.1021/ol3030023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaHSO3
2: pyridine
3: 40 percent / Bacillus sp., glucose / H2O / 48 h / 30 °C
4: LiAlH4 / diethyl ether
With
pyridine; lithium aluminium tetrahydride; D-glucose; Bacillus sp; sodium hydrogensulfite;
In
diethyl ether; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 20 °C
2: osmium(VIII) oxide; sodium periodate; 2,6-dimethylpyridine / 1,4-dioxane; water / 3 h / 20 °C
3: (+)-6,6'-(((1R,2R,4R,5R)-bicyclo[2.2.2]octane-2,5-diylbis(azanediyl))bis(methylene))bis(2,4-di-tert-butylphenol); copper(I) trifluoromethanesolfonate toluene complex / methanol / 40 °C / Molecular sieve
4: hydrogen; palladium on activated charcoal / methanol / 20 °C / 760.05 Torr
With
2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; copper(I) trifluoromethanesolfonate toluene complex; palladium on activated charcoal; (+)-6,6'-(((1R,2R,4R,5R)-bicyclo[2.2.2]octane-2,5-diylbis(azanediyl))bis(methylene))bis(2,4-di-tert-butylphenol); hydrogen; potassium carbonate;
In
1,4-dioxane; methanol; water; acetone;
3: |Henry Nitro Aldol Condensation;
DOI:10.1021/ol3030023