2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester

Base Information

Chemical Name:2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester
CAS No.:42923-56-8
Molecular Formula:C₁₅H₁₈O₆
Molecular Weight:294.304
Hs Code.:
NSC Number:152693
Nikkaji Number:J1.347.902J,J797.150H

Synonyms:NSC152693;42923-56-8;2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester;NSC-152693;(2E)-2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester

Suppliers and Price of 2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester

Chemical Property:

Vapor Pressure:2.12E-07mmHg at 25°C
Boiling Point:424.1°Cat760mmHg
Flash Point:187.2°C
Density:1.171g/cm³
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:294.11033829
Heavy Atom Count:21
Complexity:390

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C=C(CC(=O)OC)C(=O)OC)OC
Isomeric SMILES:COC1=C(C=C(C=C1)/C=C(\CC(=O)OC)/C(=O)OC)OC

Technology Process of 2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester

There total 2 articles about 2-(3,4-Dimethoxybenzylidene)succinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5507-27-7
3,4-dimethoxybenzylidenesuccinic acid

: 42923-56-8
veratrylidene-succinic acid dimethyl ester

Guidance literature:: With sulfuric acid;
DOI:10.1021/ja01571a054

Reference yield:

: 42923-56-8
veratrylidene-succinic acid dimethyl ester

Guidance literature:: Veratrylaldehyd 13a, Dimethylsuccinat, NaOCH3, HCl;

Reference yield:

: 42923-56-8
veratrylidene-succinic acid dimethyl ester

: 5701-82-6,24150-24-1,68930-18-7,119182-23-9
2,3-bis[(3,4-dimethoxyphenyl)methyl]butane

Guidance literature:: Multi-step reaction with 6 steps

1: sodium ethylate; ethanol / anschliessend Erwaermen unter Zusatz von H₂O

2: Raney nickel; aluminium; aqueous NaOH / 90 °C / Hydrogenation

3: acetic acid anhydride

4: LiAlH₄; THF

6: LiAlH₄; THF

With tetrahydrofuran; sodium hydroxide; lithium aluminium tetrahydride; ethanol; sodium ethanolate; acetic anhydride; nickel; aluminium;
DOI:10.1021/ja01571a054