4-Pyrimidinecarboxylic acid, 2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl] amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)-

Base Information

Chemical Name:4-Pyrimidinecarboxylic acid, 2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl] amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)-
CAS No.:189256-40-4
Molecular Formula:C29H25ClN4O8
Molecular Weight:592.992
Hs Code.:

4-Pyrimidinecarboxylic acid,
2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl]
amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)-

Synonyms:

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Chemical Property of 4-Pyrimidinecarboxylic acid, 2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl] amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)-

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Useful:

Technology Process of 4-Pyrimidinecarboxylic acid, 2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl] amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)-

There total 4 articles about 4-Pyrimidinecarboxylic acid, 2-(4-chloro-3-nitrophenyl)-3-[(2S)-2-[[(9H-fluoren-9-ylmethoxy)carbonyl] amino]-1-oxopropyl]hexahydro-6-oxo-, (2S,4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 189256-33-5
(2S,4S)-2-(4-Chloro-3-nitro-phenyl)-3-[(S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionyl]-6-oxo-hexahydro-pyrimidine-4-carboxylic acid tert-butyl ester

: 189256-40-4
(2S,4S)-2-(4-Chloro-3-nitro-phenyl)-3-[(S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionyl]-6-oxo-hexahydro-pyrimidine-4-carboxylic acid

Guidance literature:: With trifluoroacetic acid;
DOI:10.1021/ja9639271

Reference yield:

: 103321-50-2
9H-fluoren-9-ylmethyl [(1S)-2-chloro-1-methyl-oxoethyl]carbamate

: 189256-40-4
(2S,4S)-2-(4-Chloro-3-nitro-phenyl)-3-[(S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionyl]-6-oxo-hexahydro-pyrimidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine; benzene

2: 95 percent / TFA

With trifluoroacetic acid; In pyridine; benzene;
DOI:10.1021/ja9639271

Reference yield:

: 189256-58-4
(S)-2-{[1-(4-Chloro-3-nitro-phenyl)-meth-(E)-ylidene]-amino}-succinamic acid tert-butyl ester

: 189256-40-4
(2S,4S)-2-(4-Chloro-3-nitro-phenyl)-3-[(S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionyl]-6-oxo-hexahydro-pyrimidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine; benzene

2: 95 percent / TFA

With trifluoroacetic acid; In pyridine; benzene;
DOI:10.1021/ja9639271