2-Oxa-4,9,15-triazahexadecan-16-oic acid, 14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro- 2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)-

Base Information

Chemical Name:2-Oxa-4,9,15-triazahexadecan-16-oic acid, 14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro- 2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)-
CAS No.:189280-27-1
Molecular Formula:C46H53N3O10
Molecular Weight:807.941
Hs Code.:

2-Oxa-4,9,15-triazahexadecan-16-oic acid,
14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro-
2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)-

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Chemical Property of 2-Oxa-4,9,15-triazahexadecan-16-oic acid, 14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro- 2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)-

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Technology Process of 2-Oxa-4,9,15-triazahexadecan-16-oic acid, 14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro- 2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)-

There total 2 articles about 2-Oxa-4,9,15-triazahexadecan-16-oic acid, 14-carboxy-3-oxo-1-phenyl-9-[(phenylmethoxy)carbonyl]-7-[(tetrahydro- 2H-pyran-2-yl)oxy]-, 16-(9H-fluoren-9-ylmethyl) ester, (7R,14S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 189280-23-7
(2S,9R)-2-Amino-11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-(tetrahydropyran-2-yloxy)-7-azaundecanoic Acid

: 189280-27-1
(2S,9R)-11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2-[(9-fluorenylmethoxycarbonyl)amino]-9-(tetrahydropyran-2-yloxy)-7-azaundecanoic Acid

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jo970119z

Reference yield: 50.0%

CHCl₃/MeOH: CHCl₃/MeOH

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 189280-23-7
(2S,9R)-2-Amino-11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-9-(tetrahydropyran-2-yloxy)-7-azaundecanoic Acid

: 189280-27-1
(2S,9R)-11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2-[(9-fluorenylmethoxycarbonyl)amino]-9-(tetrahydropyran-2-yloxy)-7-azaundecanoic Acid

Guidance literature:: In sodium carbonate; N,N-dimethyl-formamide;

Reference yield: 83.0%

: 13518-40-6
L-valine tert-butylester hydrochloride

: 189280-27-1
(2S,9R)-11-[(Benzyloxycarbonyl)amino]-7-(carbobenzyloxy)-2-[(9-fluorenylmethoxycarbonyl)amino]-9-(tetrahydropyran-2-yloxy)-7-azaundecanoic Acid

: 214051-77-1
(S)-2-[(S)-6-{Benzyloxycarbonyl-[(R)-4-benzyloxycarbonylamino-2-(tetrahydro-pyran-2-yloxy)-butyl]-amino}-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-3-methyl-butyric acid tert-butyl ester

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 21h; Ambient temperature;
DOI:10.1021/jm980389p