5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)-

Base Information

Chemical Name:5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)-
CAS No.:189315-24-0
Molecular Formula:C₃₀H₂₈N₂O₈S₂
Molecular Weight:608.693
Hs Code.:

5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid,
3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-,
(4-methoxyphenyl)methyl ester, (6R,7R)-

Synonyms:

Suppliers and Price of 5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)-

There total 3 articles about 5-Thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, 3-[[(4-methylphenyl)sulfonyl]oxy]-8-oxo-7-[(phenylacetyl)amino]-, (4-methoxyphenyl)methyl ester, (6R,7R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131857-34-6
(E)-2-((2R,3R)-2-Benzenesulfonylsulfanyl-4-oxo-3-phenylacetylamino-azetidin-1-yl)-4-chloro-3-hydroxy-but-2-enoic acid 4-methoxy-benzyl ester

: 189315-24-0
8-oxo-7-phenylacetylamino-3-(toluene-4-sulfonyloxy)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 9 percent / Na₂CO₃ / dimethylformamide / 2 h / 0 °C

2: 3 percent Chromat_. / BiCl₃, Zn / dimethylformamide / 2.1 h / Ambient temperature

With bismuth(III) chloride; sodium carbonate; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/jo970051n

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 189315-24-0
8-oxo-7-phenylacetylamino-3-(toluene-4-sulfonyloxy)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 9 percent / Na₂CO₃ / dimethylformamide / 2 h / 0 °C

2: 3 percent Chromat_. / BiCl₃, Zn / dimethylformamide / 2.1 h / Ambient temperature

With bismuth(III) chloride; sodium carbonate; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/jo970051n