2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide

Base Information

Chemical Name:2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide
CAS No.:156454-78-3
Molecular Formula:C₁₁H₁₃N₂O₄P
Molecular Weight:268.209
Hs Code.:
DSSTox Substance ID:DTXSID60935460
Nikkaji Number:J582.952F
Mol file:156454-78-3.mol

Synonyms:2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide;2,3-Dihydro-2-(4-morpholinyl)-4H-1,3,2-benzoxazaphosphorin-4-one 2-oxide;4H-1,3,2-Benzoxazaphosphorin-4-one, 2,3-dihydro-2-(4-morpholinyl)-, 2-oxide;156454-78-3;C11H13N2O4P;DTXSID60935460;C11-H13-N2-O4-P;LS-41616;2-Morpholino-2H-1,3,2-benzoxazaphosphorin-4(3H)-one 2-oxide;4-Hydroxy-2-(morpholin-4-yl)-2H-1,3,2lambda~5~-benzoxazaphosphinin-2-one

Suppliers and Price of 2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.45g/cm³
XLogP3:0.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:268.06129390
Heavy Atom Count:18
Complexity:383

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1P2(=O)NC(=O)C3=CC=CC=C3O2

Technology Process of 2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide

There total 2 articles about 2-Morpholino-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-one 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 110-91-8,99108-56-2
morpholine

: 156454-74-9
2-chloro-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-on-2-oxide

: 156454-78-3
2-morpholine-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-on-2-oxide

Guidance literature:: In tetrahydrofuran; for 9h;
DOI:10.1002/ardp.19943270408

Reference yield:

: 65-45-2
salicylamide

: 156454-78-3
2-morpholine-2,3-dihydro-1,3,2-benzoxazaphosphorin-4-on-2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / POCl₃ / diethyl ether / 10 h / Heating

2: 56 percent / tetrahydrofuran / 9 h

With trichlorophosphate; In tetrahydrofuran; diethyl ether;
DOI:10.1002/ardp.19943270408