1-phenylnonan-3-ol

Base Information

• Chemical Name: 1-phenylnonan-3-ol
• CAS No.: 20452-78-2
• Molecular Formula: C₁₅H₂₄O
• Molecular Weight: 220.355
• Mol file: 20452-78-2.mol

Synonyms:

Chemical Property of 1-phenylnonan-3-ol

Chemical Property:

• Vapor Pressure: 6.6E-05mmHg at 25°C
• Boiling Point: 330.6°Cat760mmHg
• Flash Point: 125.1°C
• Density: 0.934g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-phenylnonan-3-ol

There total 13 articles about 1-phenylnonan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3-phenyl-propionaldehyde (104-53-0) + 1-Iodohexane (638-45-9) → 1-phenyl-nonan-3-ol (138298-33-6,20452-78-2)

Guidance literature:

With manganese; zirconocene dichloride; lithium chloride; cobalt(II) phthalocyanine; (3,3'-dimethyl-2,2'-dipyridyl)CrCl₃; In 1,2-dimethoxyethane; at 20 ℃; for 6h;

DOI:10.1021/ol052085k

Reference yield: 82.0%

rac-octan-2-ol (4128-31-8,113301-48-7,4128-32-9) + benzyl alcohol (100-51-6,185532-71-2) → 1-phenyl-nonan-3-ol (138298-33-6,20452-78-2) + 1-phenyl-nonan-3-one (56741-23-2)

Guidance literature:

With [Ru(P(NOH)₂)Cl₂(PPh₃)]; sodium hydroxide; In toluene; at 150 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.joc.7b02042

Reference yield: 76.0%

rac-octan-2-ol (4128-31-8,113301-48-7,4128-32-9) + benzyl alcohol (100-51-6,185532-71-2) → 1-phenyl-nonan-3-ol (138298-33-6,20452-78-2)

Guidance literature:

With C₁₇H₁₅Cl₃N₅Ru; potassium hydroxide; at 110 ℃; for 12h; under 750.075 Torr; Inert atmosphere; Sealed tube; Green chemistry;

DOI:10.1021/acs.organomet.6b00130

upstream raw materials:

3-phenyl-propionaldehyde

1-hexene

trans-1-phenyl-3-hexylpropenone

hexyl-methyl-ketone

Downstream raw materials:

1-phenylnonan-3-yl 4-methylbenzenesulfonate