Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-

Base Information

Chemical Name:Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-
CAS No.:189764-89-4
Molecular Formula:C20H18N2O4
Molecular Weight:350.374
Hs Code.:
DSSTox Substance ID:DTXSID90445547
Wikidata:Q82264001
Mol file:189764-89-4.mol

Synonyms:Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-;189764-89-4;DTXSID90445547

Suppliers and Price of Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:350.12665706
Heavy Atom Count:26
Complexity:416

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N(C2=CC=C(C=C2)OC)C3=CC(=CC=C3)[N+](=O)[O-]

Technology Process of Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro-

There total 1 articles about Benzenamine, N,N-bis(4-methoxyphenyl)-3-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 99-09-2
3-nitro-aniline

: 88849-27-8
4-methoxy-N-(3-nitrophenyl)benzenamine

: 189764-89-4
3-nitro-N,N-di(4-methoxyphenyl)benzenamine

Guidance literature:: With copper(l) iodide; potassium carbonate; pipecolic Acid; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1002/adsc.200606198

Reference yield: 100.0%

: 189764-89-4
3-nitro-N,N-di(4-methoxyphenyl)benzenamine

: 194416-43-8
N,N-Bis-(4-methoxy-phenyl)-benzene-1,3-diamine

Guidance literature:: With hydrogen; nickel; In ethanol; for 18h; Ambient temperature;

Reference yield:

: 189764-89-4
3-nitro-N,N-di(4-methoxyphenyl)benzenamine

: 194416-44-9
N,N-bis(4-methoxyphenyl)-N-3-bromophenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Raney nickel, H₂ / ethanol / 18 h / Ambient temperature

2: 1.) conc. HBr, 2.) sodium nitrite, 3.) copper(I) bromide, aq. HBr / 1) <0 deg C; 2) water, 0 deg C, 1 h 15 min; 3) water, 0 deg C, 1 h, rt --> 90 deg C

With hydrogen bromide; hydrogen; nickel; copper(I) bromide; sodium nitrite; In ethanol;