9-Phenyl-9H-fluorene-4-carbonitrile

Base Information

• Chemical Name: 9-Phenyl-9H-fluorene-4-carbonitrile
• CAS No.: 32377-09-6
• Molecular Formula: C₂₀H₁₃N
• Molecular Weight: 267.33
• DSSTox Substance ID: DTXSID60954151
• Nikkaji Number: J1.615.982D

Synonyms:9-PHENYL-9H-FLUORENE-4-CARBONITRILE;32377-09-6;DTXSID60954151

Chemical Property of 9-Phenyl-9H-fluorene-4-carbonitrile

Chemical Property:

• Vapor Pressure: 1.77E-07mmHg at 25°C
• Boiling Point: 426.4°C at 760 mmHg
• Flash Point: 213.1°C
• Density: 1.23g/cm³
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 267.104799419
• Heavy Atom Count: 21
• Complexity: 413

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2C3=CC=CC=C3C4=C(C=CC=C24)C#N

Technology Process of 9-Phenyl-9H-fluorene-4-carbonitrile

There total 3 articles about 9-Phenyl-9H-fluorene-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Cyano-9-phenyl-fluorenol → 4-Cyano-9-fluoren (32377-09-6)

Guidance literature:

With phosphorus; iodine;

DOI:10.1039/j29710000503

Reference yield:

4-cyano-9-fluorenone (4269-20-9) → 4-Cyano-9-fluoren (32377-09-6)

Guidance literature:

Multi-step reaction with 2 steps

2: phosphorus, I₂

With phosphorus; iodine;

DOI:10.1039/j29710000503

Reference yield:

phenylmagnesium bromide → 4-Cyano-9-fluoren (32377-09-6)

Guidance literature:

Multi-step reaction with 2 steps

2: phosphorus, I₂

With phosphorus; iodine;

DOI:10.1039/j29710000503

upstream raw materials:

4-cyano-9-fluorenone

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