Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro-

Base Information

• Chemical Name: Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro-
• CAS No.: 32624-91-2
• Molecular Formula: C14H12
• Molecular Weight: 180.2451
• Hs Code.: 2902199090
• DSSTox Substance ID: DTXSID50954342
• Nikkaji Number: J959.082J
• Mol file: 32624-91-2.mol

Synonyms:32624-91-2;Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro-;Cyclobuta[a]acenaphthylene, 6b,7,8,8a-tetrahydro-;6b,7,8,8a-Tetrahydrocyclobuta[a]acenaphthylene;Cyclobut[a]acenaphthylene, 6b,7,8,8a-tetrahydro-;DTXSID50954342

Chemical Property of Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro-

Chemical Property:

• Vapor Pressure: 0.000272mmHg at 25°C
• Boiling Point: 333°Cat760mmHg
• Flash Point: 163.6°C
• PSA: 0.00000
• Density: 1.19g/cm³
• LogP: 3.81440
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 180.093900383
• Heavy Atom Count: 14
• Complexity: 220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CC2C1C3=CC=CC4=C3C2=CC=C4

Technology Process of Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro-

There total 8 articles about Cyclobuta(a)acenaphthylene, 6b,7,8,8a-tetrahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

1,4-dihydro-1,4-ethanonaphtho<1,8-de><1,2>diazepine (52720-26-0) → 1,8-divinylnaphthalene (17935-66-9) + Bicyclo[3.2.0]-heptan (32624-91-2) + 7-hydroperoxy-7,8-dihydrocycloheptanaphthalene (113274-51-4) + 1H,4H-1,4-ethanonaphtho<1,8-de><1,2>dioxepin (113274-50-3)

Guidance literature:

With oxygen; In methanol; at 20 ℃; under 760 Torr; Irradiation;

DOI:10.1021/ja00216a027

Reference yield: 16.0%

1,4-dihydro-1,4-ethanonaphtho<1,8-de><1,2>diazepine (52720-26-0) → 1,8-divinylnaphthalene (17935-66-9) + Bicyclo[3.2.0]-heptan (32624-91-2)

Guidance literature:

With oxygen; In benzene; at 20 ℃; under 760 Torr; Irradiation;

DOI:10.1021/ja00216a027

Reference yield: 12.0%

1,4-dihydro-1,4-ethanonaphtho<1,8-de><1,2>diazepine (52720-26-0) → 1,8-divinylnaphthalene (17935-66-9) + Bicyclo[3.2.0]-heptan (32624-91-2) + 1H,4H-1,4-ethanonaphtho<1,8-de><1,2>dioxepin (113274-50-3)

Guidance literature:

With oxygen; In methyl cyclohexane; at 20 ℃; under 760 Torr; Irradiation;

DOI:10.1021/ja00216a027

upstream raw materials:

8,8a-dihydrocyclobutacenaphthylen-7(6bH)-one p-tolylsulphonylhydrazone

1,4-dihydro-1,4-ethanonaphtho<1,8-de><1,2>diazepine

1,8-divinylnaphthalene

C₁₄H₁₂N₂