(2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol

Base Information

Chemical Name:(2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol
CAS No.:189950-71-8
Molecular Formula:C₁₉H₂₂OSi
Molecular Weight:294.469
Hs Code.:
DSSTox Substance ID:DTXSID401240287
Mol file:189950-71-8.mol

Synonyms:DTXSID401240287;(2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol;189950-71-8

Suppliers and Price of (2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:294.143991855
Heavy Atom Count:21
Complexity:307

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC[Si](C=CCO)(C1=CC=CC=C1)C2=CC=CC=C2
Isomeric SMILES:C=CCC[Si](/C=C/CO)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of (2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol

There total 2 articles about (2E)-3-(3-Buten-1-yldiphenylsilyl)-2-propen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 89561-32-0
(but-3-enyl)diphenylsilane

: 107-19-7
propargyl alcohol

: 189950-71-8
(E)-3-(But-3-enyl-diphenyl-silanyl)-prop-2-en-1-ol

Guidance literature:: t-Bu₃P-Pt(CH₂=CH-SiMe₂-O-SiMe₂-CH=CH₂); In tetrahydrofuran; for 3h; Heating;

Reference yield:

: 1631-83-0
diphenylsilyl chloride

: 189950-71-8
(E)-3-(But-3-enyl-diphenyl-silanyl)-prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / diethyl ether

2: 77 percent / t-Bu₃P-Pt(CH₂=CH-SiMe₂-O-SiMe₂-CH=CH₂) / tetrahydrofuran / 3 h / Heating

With magnesium; t-Bu₃P-Pt(CH₂=CH-SiMe₂-O-SiMe₂-CH=CH₂); In tetrahydrofuran; diethyl ether;

Reference yield:

: 189950-71-8
(E)-3-(But-3-enyl-diphenyl-silanyl)-prop-2-en-1-ol

: 189950-72-9
(2E,4E)-5-(But-3-enyl-diphenyl-silanyl)-penta-2,4-dienoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCC / CH₂Cl₂ / 3 h / Ambient temperature

2: DCM / Heating

With 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; pyridinium chlorochromate; In dichloromethane;