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norchloroepibatidine

Base Information Edit
  • Chemical Name:norchloroepibatidine
  • CAS No.:155322-26-2
  • Molecular Formula:C11H14N2
  • Molecular Weight:174.246
  • Hs Code.:
  • Mol file:155322-26-2.mol
norchloroepibatidine

Synonyms:norchloroepibatidine

Suppliers and Price of norchloroepibatidine
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of norchloroepibatidine Edit
Chemical Property:
  • Vapor Pressure:0.000801mmHg at 25°C 
  • Boiling Point:305.8°Cat760mmHg 
  • Flash Point:138.8°C 
  • PSA:24.92000 
  • Density:1.098g/cm3 
  • LogP:2.01830 
Purity/Quality:
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MSDS Files:

SDS file from LookChem

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Technology Process of norchloroepibatidine

There total 21 articles about norchloroepibatidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With trimethylsilyl iodide; In chloroform; for 5h; Heating;
DOI:10.1002/(SICI)1099-1344(199908)42:8<761::AID-JLCR234>3.0.CO;2-S
Guidance literature:
With sodium methylate; In methanol; at 23 ℃; for 2h;
DOI:10.1021/jo00073a013
Guidance literature:
Multi-step reaction with 14 steps
1: 60 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C
2: 88 percent / PCC / CH2Cl2 / 2 h / 23 °C
3: 89 percent / KHMDS, 18-crown-6*CH3CN / tetrahydrofuran / 1 h / -78 °C
4: 95 percent / toluene / 24 h / 190 °C
5: 100 percent / LiOH / tetrahydrofuran / 5 h / 23 °C
6: Et3N, (PhO)2P(=O)N3 / toluene / 2 h / 85 °C
7: 95 percent / 12 h / 85 °C
8: TBAF / tetrahydrofuran / 4 h / 55 °C
9: Et3N / CH2Cl2 / 0.5 h / 23 °C
10: Br2, Et4N(+)Br(-) / CH2Cl2 / 0.5 h / -78 °C
11: t-BuOK / tetrahydrofuran / 18 h / -78 - 4 °C
12: Bu3SnH, AIBN / benzene / 1.5 h / Heating
13: 95 percent / NaI, AcCl / various solvent(s) / 48 h / 130 °C
14: NaOMe / methanol / 2 h / 23 °C
With lithium hydroxide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; potassium tert-butylate; tetraethylammonium bromide; tetrabutyl ammonium fluoride; bromine; tri-n-butyl-tin hydride; sodium methylate; potassium hexamethylsilazane; 18-crown-6 complexed with acetonitrile; triethylamine; acetyl chloride; pyridinium chlorochromate; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; toluene; benzene;
DOI:10.1021/jo00073a013
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