10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine

Base Information

Chemical Name:10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine
CAS No.:36065-49-3
Molecular Formula:C19H23N
Molecular Weight:0
Hs Code.:
Mol file:36065-49-3.mol

Synonyms:10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine;Dimethyl-(5-methyl-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-4-ylmethyl)-amine;

Suppliers and Price of 10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine

Chemical Property:

Vapor Pressure:5.64E-05mmHg at 25°C
Boiling Point:346.7°C at 760 mmHg
Flash Point:148°C
PSA：3.24000
Density:1.019g/cm³
LogP:3.99860

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine

There total 2 articles about 10,11-Dihydro-N,N,5-trimethyl-5H-dibenzo[a,d]cycloheptene-4-methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33953-64-9
10,11-Dihydro-N,N-dimethyl-5-methylen-5H-dibenzocyclohepten-4-methylamin

: 36065-49-3
10.11-Dihydro-N.N.5-trimethyl-5H-dibenzo[a.d]-cyclohepten-4)-methylamin

Guidance literature:: With phosphorus; hydrogen iodide; In acetic acid;
DOI:10.1021/jm00292a024

Reference yield:

: 2,2-Dimethyl-1,2,3,7,8,12b-hexahydrobenzo<6,7>cyclohepta<1,2,3-d,e>isochinolinium

: 36065-49-3
10.11-Dihydro-N.N.5-trimethyl-5H-dibenzo[a.d]-cyclohepten-4)-methylamin

Guidance literature:: Multi-step reaction with 2 steps

1: ion-exchange resin - form> / methanol; H₂O

2: aq. HI, phosphorus / acetic acid

With phosphorus; ion-exchange resin - form>; hydrogen iodide; In methanol; water; acetic acid;
DOI:10.1021/jm00292a024

Reference yield:

: 36065-49-3
10.11-Dihydro-N.N.5-trimethyl-5H-dibenzo[a.d]-cyclohepten-4)-methylamin

: 36065-50-6
3-(10.11-Dihydro-N.N.5-trimethyl-5H-dibenzo[a.d]-cyclohepten-4)-propylamin

Guidance literature:: Multi-step reaction with 4 steps

1: ClCO₂Et / benzene

3: (i) SOCl₂, DMF, (ii) /BRN= 3589311/, aq. NaOH, benzene

4: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; chloroformic acid ethyl ester; In tetrahydrofuran; benzene;
DOI:10.1021/jm00292a024