3-Iodoisopropylbenzene

Base Information

• Chemical Name: 3-Iodoisopropylbenzene
• CAS No.: 19099-56-0
• Molecular Formula: C9H11I
• Molecular Weight: 246.091
• Hs Code.: 2903999090
• Mol file: 19099-56-0.mol

Synonyms:3-Iodoisopropylbenzene;1-iodanyl-3-propan-2-yl-benzene;Benzene,1-iodo-3-(1-methylethyl);1-iodo-3-isopropylbenzene;

Chemical Property of 3-Iodoisopropylbenzene

Chemical Property:

• Vapor Pressure: 0.0939mmHg at 25°C
• Boiling Point: 227 °C(Press: 741 Torr)
• PSA: 0.00000
• Density: 1.5279 g/cm3
• LogP: 3.41460

Purity/Quality:

98%min ^*data from raw suppliers

1-Iodo-3-isopropylbenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Iodoisopropylbenzene

There total 2 articles about 3-Iodoisopropylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

meta-iso-propyl aniline (5369-16-4) → 1-iodo-3-isopropylbenzene (19099-56-0)

Guidance literature:

meta-iso-propyl aniline; With hydrogenchloride; In water; acetone; at 0 ℃; for 0.5h;

With sodium nitrite; In water; acetone; at 0 - 5 ℃; for 0.5h;

With potassium iodide; In water; acetone;

DOI:10.1002/ejoc.202100021

Reference yield:

→ 1-iodo-3-isopropylbenzene (19099-56-0)

Guidance literature:

m-Cumidin, 1) Diazotieren, 2) wss. KI, 3-5grad, 3) Δ Siedetemp.;

Reference yield: 92.0%

1-iodo-3-isopropylbenzene (19099-56-0) + propargyl alcohol (107-19-7) → 3-(3-isopropylphenyl)prop-2-yn-1-ol

Guidance literature:

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In toluene; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/ejoc.202100021

upstream raw materials:

meta-iso-propyl aniline

Downstream raw materials:

2-(3-isopropylphenyl)-6-methoxy-3,4-dihydroisoquinolin-1(2H)-one

4-[2-(3-isopropyl-phenyl)-6-methoxy-1-methyl-1,2,3,4-tetrahydro-isoquinolin-1-yl]-phenol

1-(4-benzyloxy-phenyl)-2-(3-isopropyl-phenyl)-6-methoxy-1-methyl-1,2,3,4-tetrahydro-isoquinoline

2-(3-isopropyl-phenyl)-6-methoxy-1-methyl-1-[4-(2-piperidin-1-yl-ethoxy)-phenyl]-1,2,3,4-tetrahydro-isoquinoline

Refernces