Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]-

Base Information

Chemical Name:Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]-
CAS No.:191403-45-9
Molecular Formula:C52H76Ge2
Molecular Weight:846.355
Hs Code.:
Mol file:191403-45-9.mol

Synonyms:

Suppliers and Price of Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]-

There total 1 articles about Digermene, tetrakis[6-(1,1-dimethylethyl)-2,3,4-trimethylphenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: germanium(II) chloride dioxane

: 213553-76-5
2-tert-butyl-4,5,6-trimethylphenylmagnesium bromide

: 191403-45-9
tetrakis(2-tert-butyl-4,5,6-trimethyl-phenyl)digermene

Guidance literature:: In tetrahydrofuran; (inert atmosphere); addn. at -18°C over 20 min, warming to room temp.; solvent removal, extn. (toluene), filtration, concn., crystn. on coolingto -18°C; elem. anal.;
DOI:10.1002/cber.19971300610

Reference yield: 96.0%

: 191403-45-9
tetrakis(2-tert-butyl-4,5,6-trimethyl-phenyl)digermene

: 886-66-8
1,4-diphenyl-1,3-butadiyne

: 287935-72-2
Ge₂((CH₃)3C₄H₉C₆H)4C₄(C₆H₅)2

Guidance literature:: In hexane; a mixt. in hexane was stirred at room temp. for 4 d; filtered; elem. anal.;
DOI:10.1021/om000284w

Reference yield: 90.0%

: 191403-45-9
tetrakis(2-tert-butyl-4,5,6-trimethyl-phenyl)digermene

: 28227-41-0,24764-90-7
1,4-diisopropyl-1,4-diazabuta-1,3-diene

: 881399-61-7
2,2-bis(2-tertbutyl-4,5,6-trimethylphenyl)-1,3-diisopropyl-1,3-diaza-2-germacyclopent-4-ene

Guidance literature:: In tetrahydrofuran; dropwise addn. of diazabutadiene soln. to the digermene soln., 2 d room temp., (Ar); vac. evapn., redissolving in hexane, cooling to -30 °C, recystn. (pentane), elem. anal.;
DOI:10.1002/zaac.200400527