Silanol, tris(2,4,6-trimethylphenyl)-

Base Information

• Chemical Name: Silanol, tris(2,4,6-trimethylphenyl)-
• CAS No.: 192059-69-1
• Molecular Formula: C₂₇H₃₄OSi
• Molecular Weight: 402.652
• DSSTox Substance ID: DTXSID00409337
• Nikkaji Number: J3.255.925E
• Wikidata: Q82215129
• Mol file: 192059-69-1.mol

Synonyms:Silanol, tris(2,4,6-trimethylphenyl)-;192059-69-1;Trimesitylsilanol;SCHEMBL2941823;DTXSID00409337;AKOS024433562

Chemical Property of Silanol, tris(2,4,6-trimethylphenyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 402.237892238
• Heavy Atom Count: 29
• Complexity: 437

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1)C)[Si](C2=C(C=C(C=C2C)C)C)(C3=C(C=C(C=C3C)C)C)O)C

Technology Process of Silanol, tris(2,4,6-trimethylphenyl)-

There total 1 articles about Silanol, tris(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

SiCl(2,4,6-trimethylphenyl)3 (65523-28-6) → tris(2,4,6-trimethylphenyl)silanol (192059-69-1)

Guidance literature:

With potassium hydroxide; In ethanol; water; Inert atmosphere; Reflux;

DOI:10.1021/om4003957

Reference yield: 81.0%

trimethylaluminium dimer + tris(2,4,6-trimethylphenyl)silanol (192059-69-1) → bis[tris(2,4,6-trimethylphenyl)siloxy]aluminummethyl

Guidance literature:

In toluene; byproducts: methane; under Ar; ligand in toluene added dropwise to stirred soln. of Al2Me6 (molar ratio 3.3:1) in toluene at room temp. over 5 min; stirred for 30 min; solvent removed in vac.; heated at 140°C for 18 h in vac.;

DOI:10.1021/om030589l

Reference yield: 42.0%

tris(2,4,6-trimethylphenyl)silanol (192059-69-1) + nitrogen (7727-37-9) + tris(bis(trimethylsilyl)amido)uranium(III) → [U{OSi(Mes)3}3]2(μ-η2:η2-N2) + U{OSi(Mes)3} (1446786-66-8) + C108H132O4Si4U

Guidance literature:

In hexane; at 70 ℃; for 16h; Solvent; Temperature; Inert atmosphere;

DOI:10.1021/om4003957

upstream raw materials:

SiCl(2,4,6-trimethylphenyl)3

Downstream raw materials:

Al(CH₃)2(N(CH₃)2C₆H₅)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=(Al(CH₃)2(N(CH₃)2C₆H₅)2)B(C₆F₅)4

U{OSi(Mes)3}

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