6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine

Base Information

Chemical Name:6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine
CAS No.:13491-71-9
Molecular Formula:C16H14N6
Molecular Weight:290.327
Hs Code.:
NSC Number:98710
DSSTox Substance ID:DTXSID40294921

Synonyms:13491-71-9;6-phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine;NSC98710;DTXSID40294921;NSC-98710

Suppliers and Price of 6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine

Chemical Property:

Vapor Pressure:3.6E-15mmHg at 25°C
Boiling Point:617.3°Cat760mmHg
Flash Point:327.2°C
Density:1.33g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:290.12799447
Heavy Atom Count:22
Complexity:362

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C(=NC(=N2)N)N)N=NC3=CC=CC=C3

Technology Process of 6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine

There total 4 articles about 6-Phenyl-5-[(e)-phenyldiazenyl]pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 593-85-1,90332-86-8,3425-08-9
diguanidine carbonate

: 192632-21-6
1-benzoyl-1-phenylazoacetonitrile

: 13491-71-9
2,4-diamino-5-phenylazo-6-phenylpyrimidine

Guidance literature:: at 130 ℃; for 1h;

Reference yield:

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 13491-71-9
2,4-diamino-5-phenylazo-6-phenylpyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 17 percent / EtONa / 10 h / 110 - 120 °C

2: 1.) conc. HCl, NaNO₂, 2.) Na₂CO₃, NaOAc / 1.) H₂O, 0 deg C, 2.) H₂O, EtOH, RT, 30 min

3: 49 percent / 1 h / 130 °C

With hydrogenchloride; sodium ethanolate; sodium acetate; sodium carbonate; sodium nitrite;

Reference yield:

: 614-16-4
Benzoylacetonitrile

: 13491-71-9
2,4-diamino-5-phenylazo-6-phenylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) conc. HCl, NaNO₂, 2.) Na₂CO₃, NaOAc / 1.) H₂O, 0 deg C, 2.) H₂O, EtOH, RT, 30 min

2: 49 percent / 1 h / 130 °C

With hydrogenchloride; sodium acetate; sodium carbonate; sodium nitrite;