6-Bromo-6-deoxy-D-mannitol

Base Information

Chemical Name:6-Bromo-6-deoxy-D-mannitol
CAS No.:15430-94-1
Molecular Formula:C₆H₁₃BrO₅
Molecular Weight:245.07
Hs Code.:
Mol file:15430-94-1.mol

Synonyms:Mannitol,1-bromo-1-deoxy-, D- (8CI)

Suppliers and Price of 6-Bromo-6-deoxy-D-mannitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 6-Bromo-6-deoxy-D-mannitol

Chemical Property:

Vapor Pressure:4.26E-14mmHg at 25°C
Boiling Point:543.9°C at 760 mmHg
Flash Point:282.7°C
Density:1.888g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Bromo-6-deoxy-D-mannitol

There total 5 articles about 6-Bromo-6-deoxy-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26301-79-1
D-mannono-1,4-lactone

: 15430-94-1
6-bromo-6-deoxy-D-mannitol

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / CBr₄, Ph₃P / 2 h / Ambient temperature

2: 58 percent / HClO₄ / 2 h

3: 1.) NaBH₄, ion exchange resin (IR-120, H+), 2.) AcCl / 1.) EtOH, 2.) EtOH, 5 deg C, overnight

With sodium tetrahydroborate; perchloric acid; carbon tetrabromide; ion exchange resin (IR-120; hydrogen cation; acetyl chloride; triphenylphosphine;
DOI:10.1016/S0040-4020(01)89337-6

Reference yield:

: 161085-43-4
6-bromo-6-deoxy-D-mannono-1,4-lactone

: 15430-94-1
6-bromo-6-deoxy-D-mannitol

Guidance literature:: DOI:10.1016/S0040-4020(01)89337-6

Reference yield:

: 161085-44-5
2,3,5-tri-O-acetyl-6-bromo-6-deoxy-D-mannono-1,4-lactone

: 15430-94-1
6-bromo-6-deoxy-D-mannitol

Guidance literature:: With sodium tetrahydroborate; ion exchange resin (IR-120; hydrogen cation; acetyl chloride; Yield given. Multistep reaction; 1.) EtOH, 2.) EtOH, 5 deg C, overnight;
DOI:10.1016/S0040-4020(01)89337-6