(R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt

Base Information

Chemical Name:(R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt
CAS No.:140147-97-3
Molecular Formula:C₂₉H₆₀NO₆P
Molecular Weight:549.772
Hs Code.:
Mol file:140147-97-3.mol

(R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt

Synonyms:Ethanaminium,2-[[hydroxy[[tetrahydro-2-[(octadecyloxy)methyl]-2-furanyl]methoxy]phosphinyl]oxy]-N,N,N-trimethyl-,inner salt, (R)-; (R)-SRI 62-834; MLS 266-337; SDZ 266337; SDZ-MLS 337

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Chemical Property of (R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt

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Technology Process of (R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt

There total 7 articles about (R)-2-[Hydroxy[2-(octadecyloxymethyl)tetrahydrofuran-2-ylmethoxy]phosphinyloxy]-N,N,N-trimethylethylaminium hydroxide inner salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Tetrahydro-2-<(octadecyloxy)methyl>-2-<(benzyloxy)methyl>furan

: 113201-37-9,140147-97-3
(R)-<2-<tetrahydrofuran-2-yl>methoxy>phosphinyl>oxy>ethyl>-N,N,N-trimethylaminium hydroxide inner salt

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 2534.03 Torr

2: 1.) POCl₃, Et₃N, 2.) pyridine, H₂O / 1.) THF, r.t., 2 h, 2.) 50 deg C, 5 h; 55 deg C, 5 h

With pyridine; water; hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00128a052

Reference yield:

: Tetrahydro-2-<(octadecyloxy)methyl>-2-<(benzyloxy)methyl>furan

: 113201-37-9,140147-97-3
(S)-<2-<tetrahydrofuran-2-yl>methoxy>phosphinyl>oxy>ethyl>-N,N,N-trimethylaminium hydroxide inner salt

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethanol / 2534.03 Torr

2: 1.) POCl₃, Et₃N, 2.) pyridine, H₂O / 1.) THF, r.t., 2 h, 2.) 50 deg C, 5 h; 55 deg C, 5 h

With pyridine; water; hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00128a052

Reference yield:

: Tetrahydro-2-<(octadecyloxy)metyl>-2-<(trityloxy)methyl>furan

: 113201-37-9,140147-97-3
(R)-<2-<tetrahydrofuran-2-yl>methoxy>phosphinyl>oxy>ethyl>-N,N,N-trimethylaminium hydroxide inner salt

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / aq. TFA / CH₂Cl₂ / Ambient temperature

2: 1.) POCl₃, Et₃N, 2.) pyridine, H₂O / 1.) THF, r.t., 2 h, 2.) 50 deg C, 5 h; 55 deg C, 5 h

With pyridine; water; triethylamine; trifluoroacetic acid; trichlorophosphate; In dichloromethane;
DOI:10.1021/jo00128a052