Carbamic acid, [1-[(phenylmethoxy)methyl]-7-[(tetrahydro-2H-pyran-2-yl)oxy]-2-heptenyl] [[2-(trimethylsilyl)ethyl]sulfonyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [1-[(phenylmethoxy)methyl]-7-[(tetrahydro-2H-pyran-2-yl)oxy]-2-heptenyl] [[2-(trimethylsilyl)ethyl]sulfonyl]-, 1,1-dimethylethyl ester
• CAS No.: 193612-09-8
• Molecular Formula: C30H51NO7SSi
• Molecular Weight: 597.889

Synonyms:

Chemical Property of Carbamic acid, [1-[(phenylmethoxy)methyl]-7-[(tetrahydro-2H-pyran-2-yl)oxy]-2-heptenyl] [[2-(trimethylsilyl)ethyl]sulfonyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [1-[(phenylmethoxy)methyl]-7-[(tetrahydro-2H-pyran-2-yl)oxy]-2-heptenyl] [[2-(trimethylsilyl)ethyl]sulfonyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [1-[(phenylmethoxy)methyl]-7-[(tetrahydro-2H-pyran-2-yl)oxy]-2-heptenyl] [[2-(trimethylsilyl)ethyl]sulfonyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C30H49NO7SSi → C30H51NO7SSi (193612-09-8)

Guidance literature:

With hydrogen; Pd-BaSO₄; In pyridine;

DOI:10.1016/S0040-4020(97)90397-5

Reference yield:

C30H51NO7SSi (193612-09-8) → 2-Trimethylsilanyl-ethanesulfonic acid [(Z)-1-benzyloxymethyl-7-(tetrahydro-pyran-2-yloxy)-hept-2-enyl]-amide

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;

DOI:10.1016/S0040-4020(97)90397-5

Reference yield:

C30H51NO7SSi (193612-09-8) → (Z)-8-Benzyloxymethyl-1-(2-trimethylsilanyl-ethanesulfonyl)-1,2,3,4,5,8-hexahydro-azocine

Guidance literature:

Multi-step reaction with 3 steps

1: TFA / CH₂Cl₂ / 3 h / 0 °C

2: K₂CO₃ / methanol / 16 h / Ambient temperature

3: 59 percent / Bu₃P, DEAD / tetrahydrofuran / 35 h / 0 - 25 °C

With tributylphosphine; potassium carbonate; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1016/S0040-4020(97)90397-5

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