3,5-Dibromo-2,6-dimethylpyridin-4-amine

Base Information

• Chemical Name: 3,5-Dibromo-2,6-dimethylpyridin-4-amine
• CAS No.: 193690-72-1
• Molecular Formula: C7H8Br2N2
• Molecular Weight: 279.962
• DSSTox Substance ID: DTXSID20443511
• Mol file: 193690-72-1.mol

Synonyms:3,5-Dibromo-2,6-dimethylpyridin-4-amine;193690-72-1;4-Pyridinamine, 3,5-dibromo-2,6-dimethyl-;SCHEMBL21963176;DTXSID20443511;W19400

Chemical Property of 3,5-Dibromo-2,6-dimethylpyridin-4-amine

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 279.90337
• Heavy Atom Count: 11
• Complexity: 128

Purity/Quality:

95+% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=C(C(=N1)C)Br)N)Br

Technology Process of 3,5-Dibromo-2,6-dimethylpyridin-4-amine

There total 1 articles about 3,5-Dibromo-2,6-dimethylpyridin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-amino-2,6-lutidine (3512-80-9) → 3-bromo-4-amino-2,6-dimethylpyridine (33259-24-4) + 4-amino-3,5-dibromo-2,6-dimethylpyridine (193690-72-1)

Guidance literature:

With bromine; acetic acid; for 1h; Ambient temperature;

DOI:10.1002/jhet.5570340303

Reference yield: 100.0%

4-amino-3,5-dibromo-2,6-dimethylpyridine (193690-72-1) + (2-ethoxyphenyl)boronic acid (213211-69-9) → 4-amino-3,5-di-(2-ethoxyphenyl)-2,6-dimethylpyridine

Guidance literature:

With potassium phosphate; 2-dicyclohexylphosphino-2′,6′-dimethoxybiphenyl; palladium diacetate; In toluene; at 90 ℃; for 0.116667h; Inert atmosphere;

DOI:10.1002/ejoc.201600456

Reference yield: 100.0%

4-amino-3,5-dibromo-2,6-dimethylpyridine (193690-72-1) + 2-Methoxyphenylboronic acid (5720-06-9) → (M,P)-4-amino-3,5-bis(2-methoxyphenyl)-2,6-dimethylpyridine

Guidance literature:

With potassium phosphate; 2-dicyclohexylphosphino-2′,6′-dimethoxybiphenyl; palladium diacetate; In toluene; at 90 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/ejoc.201600456

upstream raw materials:

4-amino-2,6-lutidine

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