Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester

Base Information

Chemical Name:Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester
CAS No.:193806-57-4
Molecular Formula:C24H29NO4S
Molecular Weight:427.565
Hs Code.:
Mol file:193806-57-4.mol

Synonyms:

Suppliers and Price of Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester

There total 7 articles about Benzenecarbothioic acid, 2-[(2-methyl-2-propenyl)oxy]-, S-[2-[2-[[(1,1-dimethylethoxy)carbonyl]amino]phenyl]ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121767-60-0
2-methallyloxybenzoyl chloride

: 193806-48-3
[2-(2-Mercapto-ethyl)-phenyl]-carbamic acid tert-butyl ester

: 193806-57-4
2-(2-Methyl-allyloxy)-thiobenzoic acid S-[2-(2-tert-butoxycarbonylamino-phenyl)-ethyl] ester

Guidance literature:: With dmap; In dichloromethane; Ambient temperature;
DOI:10.1021/jo970500j

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 193806-57-4
2-(2-Methyl-allyloxy)-thiobenzoic acid S-[2-(2-tert-butoxycarbonylamino-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / NaHCO₃ / dioxane; H₂O / 4 h / Ambient temperature

2: 99 percent / Et₃N / tetrahydrofuran / 0.33 h / -30 °C

3: 96 percent / dimethylformamide / 14 h / Ambient temperature

4: 92 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

5: 80 percent / DMAP / CH₂Cl₂ / Ambient temperature

With dmap; lithium aluminium tetrahydride; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo970500j

Reference yield:

: 5339-85-5
2-aminophenethyl alcohol

: 193806-57-4
2-(2-Methyl-allyloxy)-thiobenzoic acid S-[2-(2-tert-butoxycarbonylamino-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / NaHCO₃ / dioxane; H₂O / 4 h / Ambient temperature

2: 99 percent / Et₃N / tetrahydrofuran / 0.33 h / -30 °C

3: 96 percent / dimethylformamide / 14 h / Ambient temperature

4: 92 percent / LiAlH₄ / diethyl ether / 1.5 h / 0 °C

5: 80 percent / DMAP / CH₂Cl₂ / Ambient temperature

With dmap; lithium aluminium tetrahydride; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo970500j