Benzenepropanoic acid, 4-(phenylmethyl)-, methyl ester

Base Information

Chemical Name:Benzenepropanoic acid, 4-(phenylmethyl)-, methyl ester
CAS No.:193819-67-9
Molecular Formula:C17H18O2
Molecular Weight:254.329
Hs Code.:

Synonyms:

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Chemical Property of Benzenepropanoic acid, 4-(phenylmethyl)-, methyl ester

Chemical Property:

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Technology Process of Benzenepropanoic acid, 4-(phenylmethyl)-, methyl ester

There total 4 articles about Benzenepropanoic acid, 4-(phenylmethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 262425-93-4
methyl (2E)-3-[4-(phenylmethyl)phenyl]-2-propenoate

: 193819-67-9
3-(4-benzyl-phenyl)-propionic acid methyl ester

Guidance literature:: With hydrogen; nickel; In methanol; for 0.25h; under 258.581 Torr;
DOI:10.1021/jm990496z

Reference yield:

: 620-86-0
4-Benzylbenzoic acid

: 193819-67-9
3-(4-benzyl-phenyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride / 2 h / 25 °C

2: H₂; 2,6-lutidine / 10percent Pd/C / tetrahydrofuran / 6 h / 258.58 Torr

3: tetrahydrofuran / 10 h / Heating

4: 100 percent / H₂ / Raney nickel / methanol / 0.25 h / 258.58 Torr

With 2,6-dimethylpyridine; oxalyl dichloride; hydrogen; nickel; In tetrahydrofuran; methanol; 1: Chlorination / 2: Hydrogenation / 3: Condensation / 4: Hydrogenation;
DOI:10.1021/jm990496z

Reference yield:

: 22746-83-4
4-benzylbenzoyl chloride

: 193819-67-9
3-(4-benzyl-phenyl)-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂; 2,6-lutidine / 10percent Pd/C / tetrahydrofuran / 6 h / 258.58 Torr

2: tetrahydrofuran / 10 h / Heating

3: 100 percent / H₂ / Raney nickel / methanol / 0.25 h / 258.58 Torr

With 2,6-dimethylpyridine; hydrogen; nickel; In tetrahydrofuran; methanol; 1: Hydrogenation / 2: Condensation / 3: Hydrogenation;
DOI:10.1021/jm990496z