3,4-xylyl chloroformate

Base Information

• Chemical Name: 3,4-xylyl chloroformate
• CAS No.: 36018-20-9
• Molecular Formula: C9H9 Cl O2
• Molecular Weight: 184.622
• Hs Code.: 2915900090
• Mol file: 36018-20-9.mol

Synonyms:Formicacid, chloro-, 3,4-xylyl ester (6CI); 3,4-Dimethylphenyl chloroformate;3,4-Xylyl chloroformate; Chloroformic acid 3,4-dimethylphenyl ester

Chemical Property of 3,4-xylyl chloroformate

Chemical Property:

• Vapor Pressure: 0.044mmHg at 25°C
• Boiling Point: 237.618°C at 760 mmHg
• Flash Point: 103.025°C
• PSA: 26.30000
• Density: 1.195g/cm³
• LogP: 3.04100

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-xylyl chloroformate

There total 2 articles about 3,4-xylyl chloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-Dimethylphenol (95-65-8) + bis(trichloromethyl) carbonate (32315-10-9) → 3,4-xylyl chloroformate (36018-20-9)

Guidance literature:

With N,N-dimethyl-aniline; In tetrahydrofuran; at 5 - 20 ℃; for 3.16667h;

Reference yield:

→ 3,4-xylyl chloroformate (36018-20-9)

Guidance literature:

3,4-Dimethylphenol, Phosgen;

Reference yield: 74.0%

N1-[2-(4-cyanophenoxy)-1-methylethyl]-L-valinamide + 3,4-xylyl chloroformate (36018-20-9) → N1-[2-(4-cyanophenoxy)-1-methylethyl]-N2-(3,4-dimethylphenoxycarbonyl)-L-valinamide

Guidance literature:

With 4-methyl-morpholine; In dichloromethane;

upstream raw materials:

3,4-Dimethylphenol

bis(trichloromethyl) carbonate

Downstream raw materials:

C₁₉H₂₂N₂O₂

α,α'-Dichlor-3,4-xylenylchlorformiat

α,α'-Dichlor-3,4-xylenyl N-methylcarbamat

α,α'-Dichlor-3,4-xylenyl-N-cyclohexylcarbamat

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