Technology Process of Benzaldehyde, 2-(1-phenylethoxy)-
There total 5 articles about Benzaldehyde, 2-(1-phenylethoxy)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Schwartz's reagent;
In
tetrahydrofuran;
at 20 ℃;
for 6h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/anie.201913930
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-Adamantanecarboxylic acid; sodium 1-adamantanecarboxylate; tetrabutylammonium perchlorate; C32H21N4NiO2 / N,N-dimethyl acetamide / 12 h / 130 °C / Electrochemical reaction
2: Schwartz's reagent / tetrahydrofuran / 6 h / 20 °C / Schlenk technique; Inert atmosphere
With
Schwartz's reagent; 1-Adamantanecarboxylic acid; C32H21N4NiO2; tetrabutylammonium perchlorate; sodium 1-adamantanecarboxylate;
In
tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1002/anie.201913930
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (1,2-dimethoxyethane)dichloronickel(II); 1-Adamantanecarboxylic acid; sodium 1-adamantanecarboxylate; tetrabutylammonium perchlorate / N,N-dimethyl acetamide / 12 h / 130 °C / Inert atmosphere; Electrochemical reaction
2: Schwartz's reagent / tetrahydrofuran / 6 h / 20 °C / Schlenk technique; Inert atmosphere
With
Schwartz's reagent; (1,2-dimethoxyethane)dichloronickel(II); 1-Adamantanecarboxylic acid; tetrabutylammonium perchlorate; sodium 1-adamantanecarboxylate;
In
tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1002/anie.201913930