dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene

Base Information

Chemical Name:dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene
CAS No.:50537-29-6
Molecular Formula:C18H17N
Molecular Weight:247.3343
Hs Code.:
DSSTox Substance ID:DTXSID90964763
Nikkaji Number:J3.269.154D

Synonyms:dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene;(+-)-10,11-Dihydro-12-(2-propenyl)-5H-dibenzo(a,d)cyclohepten-5,10-imine;5H-Dibenzo(a,d)cyclohepten-5,10-imine, 10,11-dihydro-12-(2-propenyl)-, (+-)-;50537-29-6;DTXSID90964763;LS-60788;10,11-Dihydro-5,10-(2-propenylimino)-5H-dibenzo[a,d]cycloheptene;12-(Prop-2-en-1-yl)-10,11-dihydro-5H-5,10-epiminodibenzo[a,d][7]annulene

Suppliers and Price of dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene

Chemical Property:

Vapor Pressure:0.000149mmHg at 25°C
Boiling Point:332.1°Cat760mmHg
Flash Point:140.4°C
Density:1.11g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:247.136099547
Heavy Atom Count:19
Complexity:350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCN1C2CC3=CC=CC=C3C1C4=CC=CC=C24

Technology Process of dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene

There total 3 articles about dl-12-Allyl-10,11-dihydro-5,10-imino-(5H)-dibenzo(a,d)cycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 10-Allylamino-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-ol

: 50537-29-6
N-allyl-10,11-dihydro-5H-dibenzocyclohepten-5,10-imine

Guidance literature:: With acetic acid; at 100 ℃; for 5h;
DOI:10.1246/bcsj.68.3169

Reference yield:

: 10354-00-4
5H-dibenzo[a,d]cyclohepten-5-ol

: 50537-29-6
N-allyl-10,11-dihydro-5H-dibenzocyclohepten-5,10-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / p-dicyanobenzene / acetonitrile; H₂O / 8 h / Irradiation

2: 78 percent / CH₃COOH / 5 h / 100 °C

With terephthalonitrile; acetic acid; In water; acetonitrile;
DOI:10.1246/bcsj.68.3169