1,2-Hydrazinedicarboxylic acid, 1-(2-methylbutyl)-, 2-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Base Information

Chemical Name:1,2-Hydrazinedicarboxylic acid, 1-(2-methylbutyl)-, 2-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-
CAS No.:194664-31-8
Molecular Formula:C18H28N2O4
Molecular Weight:336.431
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Hydrazinedicarboxylic acid, 1-(2-methylbutyl)-, 2-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Chemical Property:

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Technology Process of 1,2-Hydrazinedicarboxylic acid, 1-(2-methylbutyl)-, 2-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

There total 5 articles about 1,2-Hydrazinedicarboxylic acid, 1-(2-methylbutyl)-, 2-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 194664-28-3
C₂₅H₃₁N₃O₆S

: 194664-31-8
C₁₈H₂₈N₂O₄

Guidance literature:: With aluminum amalgam; carbon dioxide; water; In diethyl ether;
DOI:10.1039/a703008h

Reference yield:

: 1565-80-6
(2S)-2-methyl-1-butanol

: 194664-31-8
C₁₈H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PPh₃, DEAD / tetrahydrofuran

2: 94 percent / Al(Hg), CO₂, H₂O / diethyl ether

With aluminum amalgam; carbon dioxide; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether;
DOI:10.1039/a703008h

Reference yield:

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 194664-31-8
C₁₈H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / pyridine

2: 93 percent / DMAP / acetonitrile

3: 80 percent / PPh₃, DEAD / tetrahydrofuran

4: 94 percent / Al(Hg), CO₂, H₂O / diethyl ether

With pyridine; dmap; aluminum amalgam; carbon dioxide; water; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1039/a703008h