1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-

Base Information

Chemical Name:1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-
CAS No.:67508-88-7
Molecular Formula:C29H33NO10
Molecular Weight:555.573
Hs Code.:
Mol file:67508-88-7.mol

1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-

Synonyms:

Suppliers and Price of 1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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American Custom Chemicals Corporation
1-NAPHTHACENECARBOXYLIC ACID, 1,2,3,4,6,11-HEXAHYDRO-6,11-DIOXO-2-ETHY L-4-((2,3,6-TRIDEOXY-3-AMINO-ALPHA-L-LYXO-HEXOPYRANOSYL)OXY)-2,5,7-TRI HYDROXY-, METHYL ESTER, (1R-(1-ALPHA,2-BETA,4-BETA))- 95.00%
5MG
$ 500.62

Total 0 raw suppliers

Chemical Property of 1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-

Chemical Property:

Vapor Pressure:1.05E-21mmHg at 25°C
Boiling Point:719.1°Cat760mmHg
Flash Point:388.7°C
Density:1.47g/cm³

Purity/Quality:: 1-NAPHTHACENECARBOXYLIC ACID, 1,2,3,4,6,11-HEXAHYDRO-6,11-DIOXO-2-ETHY L-4-((2,3,6-TRIDEOXY-3-AMINO-ALPHA-L-LYXO-HEXOPYRANOSYL)OXY)-2,5,7-TRI HYDROXY-, METHYL ESTER, (1R-(1-ALPHA,2-BETA,4-BETA))- 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))-

There total 23 articles about 1-Naphthacenecarboxylic acid, 1,2,3,4,6,11-hexahydro-6,11-dioxo-2-ethy l-4-((2,3,6-trideoxy-3-amino-alpha-L-lyxo-hexopyranosyl)oxy)-2,5,7-tri hydroxy-, methyl ester, (1R-(1-alpha,2-beta,4-beta))- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78773-24-7,78822-00-1
(1R,2R,4S)-2-Ethyl-2,5,7-trihydroxy-4-[(2R,4S,5S,6S)-6-methyl-4-[methyl-(2,2,2-trifluoro-acetyl)-amino]-5-(4-nitro-benzoyloxy)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacene-1-carboxylic acid methyl ester

: 65222-75-5,67508-88-7
N-demethylaklavin

: 65222-75-5,67508-88-7
(1S,2R,4S)-2-Ethyl-2,5,7-trihydroxy-4-((2R,4S,5S,6S)-5-hydroxy-6-methyl-4-methylamino-tetrahydro-pyran-2-yloxy)-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacene-1-carboxylic acid methyl ester

Guidance literature:: With sodium methylate; In methanol; at -20 ℃; for 2h;
DOI:10.1021/ja00404a047

Reference yield:

: 78773-24-7,78822-00-1
(1R,2R,4S)-2-Ethyl-2,5,7-trihydroxy-4-[(2R,4S,5S,6S)-6-methyl-4-[methyl-(2,2,2-trifluoro-acetyl)-amino]-5-(4-nitro-benzoyloxy)-tetrahydro-pyran-2-yloxy]-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacene-1-carboxylic acid methyl ester

: 65222-75-5,67508-88-7
N-demethylaklavin

: 65222-75-5,67508-88-7
(1S,2R,4S)-2-Ethyl-2,5,7-trihydroxy-4-((2R,4S,5S,6S)-5-hydroxy-6-methyl-4-methylamino-tetrahydro-pyran-2-yloxy)-6,11-dioxo-1,2,3,4,6,11-hexahydro-naphthacene-1-carboxylic acid methyl ester

Guidance literature:: With sodium methylate; In methanol; at -20 ℃; for 2h;
DOI:10.1021/ja00404a047

Reference yield:

: 78773-17-8,78773-18-9,78773-19-0,78773-20-3
9-epi-aklavinone 7-methyl ether

: 65222-75-5,67508-88-7
N-demethylaklavin

Guidance literature:: Multi-step reaction with 4 steps

1: 11 percent / potassium carbonate / methanol / 1.75 h / 65 °C

2: trifluoroacetic acid / Ambient temperature

3: 30 percent / p-toluenesulfonic acid monohydrate / benzene / 50 °C

4: sodium methoxide / methanol / 2 h / -20 °C

With sodium methylate; potassium carbonate; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; benzene;
DOI:10.1021/ja00404a047