Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester
CAS No.:195299-04-8
Molecular Formula:C18H29NO5
Molecular Weight:339.432
Hs Code.:
DSSTox Substance ID:DTXSID401115597
Mol file:195299-04-8.mol

Synonyms:DTXSID401115597;195299-04-8;Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester

Suppliers and Price of Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:339.20457303
Heavy Atom Count:24
Complexity:380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)OCC1=C(C=CC(=C1CNC(=O)OC(C)(C)C)OC)OC

Technology Process of Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester

There total 3 articles about Carbamic acid, [[3,6-dimethoxy-2-[(1-methylethoxy)methyl]phenyl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 195299-08-2
2-Azidomethyl-3-isopropoxymethyl-1,4-dimethoxy-benzene

: 195299-04-8
(2-Isopropoxymethyl-3,6-dimethoxy-benzyl)-carbamic acid tert-butyl ester

Guidance literature:: With hydrogen; In methanol; for 2h; under 760 Torr; Ambient temperature;
DOI:10.1021/jo962172d

Reference yield:

: 195299-07-1
2-Bromomethyl-3-isopropoxymethyl-1,4-dimethoxy-benzene

: 195299-04-8
(2-Isopropoxymethyl-3,6-dimethoxy-benzyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaN₃ / dimethylformamide / 2 h / Ambient temperature; other solvent

2: 87 percent / H₂ / methanol / 2 h / 760 Torr / Ambient temperature

With sodium azide; hydrogen; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo962172d

Reference yield:

: 195299-06-0
(2-Isopropoxymethyl-3,6-dimethoxy-phenyl)-methanol

: 195299-04-8
(2-Isopropoxymethyl-3,6-dimethoxy-benzyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.17 g / CBr₄, PPh₃ / tetrahydrofuran / 0.5 h / Ambient temperature

2: 100 percent / NaN₃ / dimethylformamide / 2 h / Ambient temperature; other solvent

3: 87 percent / H₂ / methanol / 2 h / 760 Torr / Ambient temperature

With sodium azide; carbon tetrabromide; hydrogen; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo962172d