ethyl 6,7-dimethoxy-3-methyl-1H-indene-2-carboxylate

Base Information

• Chemical Name: ethyl 6,7-dimethoxy-3-methyl-1H-indene-2-carboxylate
• CAS No.: 5415-54-3
• Molecular Formula: C₁₅H₁₈O₄
• Molecular Weight: 262.306
• Mol file: 5415-54-3.mol

Synonyms:Indene-2-carboxylicacid, 6,7-dimethoxy-3-methyl-, ethyl ester (6CI,8CI); NSC 10164; NSC 117500

Chemical Property of ethyl 6,7-dimethoxy-3-methyl-1H-indene-2-carboxylate

Chemical Property:

• Vapor Pressure: 4.35E-06mmHg at 25°C
• Boiling Point: 383.6°Cat760mmHg
• Flash Point: 168.9°C
• Density: 1.14g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 6,7-dimethoxy-3-methyl-1H-indene-2-carboxylate

There total 2 articles about ethyl 6,7-dimethoxy-3-methyl-1H-indene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

Ethyl 2-acetyl-3-(2,3-dimethoxyphenyl)-propanoate (53608-80-3) → 6,7-Dimethoxy-2-ethoxycarbonyl-3-methylindene (5415-54-3)

Guidance literature:

With PPA; In xylene; at 60 ℃; for 0.5h;

DOI:10.1055/s-1980-28974

Reference yield:

→ 6,7-Dimethoxy-2-ethoxycarbonyl-3-methylindene (5415-54-3)

Guidance literature:

upstream raw materials:

Ethyl 2-acetyl-3-(2,3-dimethoxyphenyl)-propanoate