Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)-

Base Information

Chemical Name:Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)-
CAS No.:19715-32-3
Molecular Formula:C14H21Br
Molecular Weight:269.225
Hs Code.:

Synonyms:2,6-di-t-butylbromobenzene;2,6-Di-tert-butylbrombenzol;2-Bromo-1,3-di-tert-butyl-benzene;1-Brom-2,6-di-tert-butyl-benzol;

Suppliers and Price of Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
1-Bromo-2,6-di-tert-butylbenzene
1g
$ 1460.20

Alichem
1-Bromo-2,6-di-tert-butylbenzene
500mg
$ 839.45

Alichem
1-Bromo-2,6-di-tert-butylbenzene
250mg
$ 475.20

AK Scientific
2-Bromo-1,3-di-tert-butylbenzene
1g
$ 2085.00

Total 0 raw suppliers

Chemical Property of Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)-

Chemical Property:

Boiling Point:264.2±9.0 °C(Predicted)
PSA：0.00000
Density:1.126±0.06 g/cm3(Predicted)
LogP:5.04410

Purity/Quality:: 1-Bromo-2,6-di-tert-butylbenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)-

There total 8 articles about Benzene, 2-bromo-1,3-bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 516526-99-1
2-bromo-1,3-bis(1-formyl-1-methylethyl)benzene

: 19715-32-3
2-bromo-1,3-di-tert-butylbenzene

Guidance literature:: With hydrazine hydrate; potassium hydroxide; In water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; at 120 - 200 ℃; for 4h;

Reference yield:

: 19715-30-1
2,6-di-t-butyl-4-nitrobromobenzene

: 19715-32-3
2-bromo-1,3-di-tert-butylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Ra-Ni

2: 1.) HNO₂ H₂SO₄ 2.) H₃PO₂

With sulfuric acid; hydrogen; hypophosphorous acid; cis-nitrous acid; Ra-Ni;
DOI:10.1016/S0040-4039(01)80586-4

Reference yield:

: 516526-98-0
2-bromo-1,3-bis(1-cyano-1-methylethyl)benzene

: 19715-32-3
2-bromo-1,3-di-tert-butylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIBAH / benzene; hexane / 0 - 20 °C

1.2: 92 percent / aq. H₂SO₄ / benzene; hexane / 2 h / 20 °C

2.1: 70 percent / H₂NNH₂*H₂O; KOH / triethylene glycol; H₂O / 6 h / 130 - 200 °C

With potassium hydroxide; diisobutylaluminium hydride; hydrazine hydrate; In hexane; water; benzene; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; 2.1: Wolff-Kishner reduction;
DOI:10.1246/bcsj.78.1110