Benzyl (4-phenylbutanoyl)carbamate

Base Information

Chemical Name:Benzyl (4-phenylbutanoyl)carbamate
CAS No.:197173-15-2
Molecular Formula:C18H19NO3
Molecular Weight:297.354
Hs Code.:
DSSTox Substance ID:DTXSID70571373
Nikkaji Number:J1.633.011F
Wikidata:Q82459446

Synonyms:Benzyl (4-phenylbutanoyl)carbamate;197173-15-2;DTXSID70571373

Suppliers and Price of Benzyl (4-phenylbutanoyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzyl (4-phenylbutanoyl)carbamate

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:297.13649347
Heavy Atom Count:22
Complexity:344

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCCC(=O)NC(=O)OCC2=CC=CC=C2

Technology Process of Benzyl (4-phenylbutanoyl)carbamate

There total 1 articles about Benzyl (4-phenylbutanoyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-84-1
O-benzyl carbamate

: 18496-54-3
phenylbutyric acid chloride

: 197173-15-2
(4-phenylbutyryl)carbamic acid benzyl ester

Guidance literature:: In toluene; at 80 ℃; for 6h;
DOI:10.1021/jo010370l

Reference yield:

: 197173-15-2
(4-phenylbutyryl)carbamic acid benzyl ester

: 197173-25-4
(1-Hydroxy-4-phenyl-butyl)-carbamic acid benzyl ester

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 1.5h; Yield given;
DOI:10.1016/S0040-4039(97)01531-1

Reference yield:

: 197173-15-2
(4-phenylbutyryl)carbamic acid benzyl ester

: (1,2,3,4-tetrahydronaphthalen-1-yl)carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL / CH₂Cl₂; toluene / -78 °C

2: TiCl₄ / CH₂Cl₂ / 1 h / -78 °C

With titanium tetrachloride; diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.1021/jo010370l